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Chemical Structure| 7515-42-6 Chemical Structure| 7515-42-6

Structure of 7515-42-6

Chemical Structure| 7515-42-6

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Product Details of [ 7515-42-6 ]

CAS No. :7515-42-6
Formula : C12H14O2
M.W : 190.24
SMILES Code : CC(OCC/C=C/C1=CC=CC=C1)=O

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Application In Synthesis of [ 7515-42-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 7515-42-6 ]

[ 7515-42-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 127-19-5 ]
  • [ 1007-03-0 ]
  • [ 7515-42-6 ]
YieldReaction ConditionsOperation in experiment
56% With copper(ll) bromide; at 140℃; for 12h;Sealed tube; General procedure: The cyclopropanemethanols 1 (1 equiv., 0.3 mmol), CuBr 2 (10 mol%, 0.03 mmol), were mixed in DMF (2 mL) were stirred at 140 o C in a sealed tube for 12 h (TLC monitored). Then the reaction mixture was cooled to room temperature. And the reaction mixture was extracted with ethyl acetate and washed with saturated brine, the organic phase was combined and dried with anhydrous Na 2 SO 4 . The solvent was evaporated to in vacuo, the crude product was purified by column chromatography, eluting with petroleum ether/EtOAc (40:1) to afford the desired 2.
 

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