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Chemical Structure| 755034-05-0 Chemical Structure| 755034-05-0

Structure of 755034-05-0

Chemical Structure| 755034-05-0

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Product Details of [ 755034-05-0 ]

CAS No. :755034-05-0
Formula : C16H13ClN2O6
M.W : 364.74
SMILES Code : O=C(OC)C1=CC=C(Cl)C=C1NC2=CC(C(OC)=O)=CC=C2[N+]([O-])=O

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Application In Synthesis of [ 755034-05-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 755034-05-0 ]

[ 755034-05-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 99512-09-1 ]
  • [ 181765-85-5 ]
  • [ 755034-05-0 ]
YieldReaction ConditionsOperation in experiment
With caesium carbonate;1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; In toluene; at 95℃; for 16h; Example 45Bmethyl 4-chloro-2-(5-(methoxycarbonyl)-2-nitrophenylamino)benzoate 2470 A solution of Example 3 A (5.35 g, 18.04 mmol), methyl 3-amino-4-nitrobenzoate(3.54 g, 18.04 mmol), CsC03 (5.88 g, 18.04 mmol), palladium(II) acetate (0.202 g, 0.902 mmol) and 1 , 1 '-bis(diphenylphosphino)ferrocene ( 1.0 g, 1.804 mmol) in toluene was heated at 95C for 16 hours. The reaction mixture was brought to 80C; filtered through a plug of silica gel and washed with ethyl acetate. The solvent was removed and residue 2475 was purified over silica gel. The material was collected and washed with minimumamount of hot ethanol to yield the title compound. MS ESI(+) m/z 365 [M+H]+.
 

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[ 755034-05-0 ]

Chemical Structure| None

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