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Chemistry
Organic Building Blocks
Aryls
(4-Bromobenzyl)(phenyl)sulfane
Chemistry
Organic Building Blocks
Aryls
Bromides Sulfides

[ CAS No. 75954-35-7 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 75954-35-7
Chemical Structure| 75954-35-7
Structure of 75954-35-7 * Storage: {[proInfo.prStorage]}
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Product Details of [ 75954-35-7 ]

CAS No. :75954-35-7 MDL No. :MFCD00471947
Formula : C13H11BrS Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 279.20 Pubchem ID :-
Synonyms :

Safety of [ 75954-35-7 ]

Signal Word: Class:
Precautionary Statements: UN#:
Hazard Statements: Packing Group:

Application In Synthesis of [ 75954-35-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 75954-35-7 ]

[ 75954-35-7 ] Synthesis Path-Downstream   1~31

  • 1
  • [ 75954-35-7 ]
  • [ 91110-68-8 ]
Reference： [1]Canadian Journal of Chemistry,2005,vol. 83,p. 115 - 121
[2]Canadian Journal of Chemistry,2007,vol. 85,p. 7 - 11
[3]Phosphorus, Sulfur and Silicon and the Related Elements,2012,vol. 187,p. 321 - 326
[4]Phosphorus, Sulfur and Silicon and the Related Elements,2005,vol. 180,p. 2751 - 2766
[5]Applied Organometallic Chemistry,2018,vol. 32
[6]Journal of the Science of Food and Agriculture,1957,vol. 8,p. 566,567
  • 2
  • [ 75954-35-7 ]
  • [ 100375-00-6 ]
Reference： [1]Phosphorus, Sulfur and Silicon and the Related Elements,2005,vol. 180,p. 2751 - 2766
[2]Canadian Journal of Chemistry,2007,vol. 85,p. 7 - 11
[3]E-Journal of Chemistry,2012,vol. 9,p. 863 - 868
[4]Canadian Journal of Chemistry,2005,vol. 83,p. 115 - 121
[5]Journal of Organic Chemistry,2011,vol. 76,p. 9593 - 9601
[6]Journal of the Science of Food and Agriculture,1957,vol. 8,p. 566,567
[7]Applied Organometallic Chemistry,2018,vol. 32
  • 3
  • [ 589-15-1 ]
  • [ 75954-35-7 ]
Reference： [1]Bulletin of the Chemical Society of Japan,1987,vol. 60,p. 4061 - 4066
[2]Organic Letters,2014,vol. 16,p. 1196 - 1199
  • 4
  • [ 16532-79-9 ]
  • [ 930-69-8 ]
  • [ 3699-01-2 ]
  • [ 6317-59-5 ]
  • [ 75954-35-7 ]
Reference： [1]Russian Journal of Organic Chemistry,1994,vol. 30,p. 435 - 441
    Zhurnal Organicheskoi Khimii,1994,vol. 30,p. 404 - 410
  • 5
  • [ 75954-35-7 ]
  • [ 106-38-7 ]
  • [ 19829-56-2 ]
Reference： [1]Journal of Organic Chemistry,1988,vol. 53,p. 2536 - 2539
  • 6
  • [ 1515-88-4 ]
  • [ 930-69-8 ]
  • [ 538-86-3 ]
  • [ 139-66-2 ]
  • [ 94306-40-8 ]
  • [ 3699-01-2 ]
  • [ 75954-35-7 ]
  • Methyl 4-phenylthiobenzyl ether [ No CAS ]
Reference： [1]Russian Journal of Organic Chemistry,1997,vol. 33,p. 1601 - 1607
  • 7
  • [ 1515-88-4 ]
  • [ 930-69-8 ]
  • [ 538-86-3 ]
  • [ 3699-01-2 ]
  • [ 75954-35-7 ]
  • Methyl 4-phenylthiobenzyl ether [ No CAS ]
Reference： [1]Russian Journal of Organic Chemistry,1997,vol. 33,p. 1601 - 1607
[2]Russian Journal of Organic Chemistry,1997,vol. 33,p. 1601 - 1607
  • 8
  • [ 20600-29-7 ]
  • [ 139-66-2 ]
  • [ 94306-40-8 ]
  • [ 946-80-5 ]
  • [ 75954-35-7 ]
Reference： [1]Russian Journal of Organic Chemistry,1997,vol. 33,p. 1601 - 1607
  • 9
  • [ 20600-22-0 ]
  • [ 930-69-8 ]
  • [ 139-66-2 ]
  • [ 94306-40-8 ]
  • [ 946-80-5 ]
  • [ 3699-01-2 ]
  • [ 75954-35-7 ]
  • Phenyl 4-phenylthiobenzyl ether [ No CAS ]
Reference： [1]Russian Journal of Organic Chemistry,1997,vol. 33,p. 1601 - 1607
  • 10
  • [ 20600-22-0 ]
  • [ 930-69-8 ]
  • [ 139-66-2 ]
  • [ 94306-40-8 ]
  • [ 3699-01-2 ]
  • [ 75954-35-7 ]
Reference： [1]Russian Journal of Organic Chemistry,1997,vol. 33,p. 1601 - 1607
[2]Russian Journal of Organic Chemistry,1997,vol. 33,p. 1601 - 1607
  • 11
  • [ 20600-22-0 ]
  • [ 930-69-8 ]
  • [ 139-66-2 ]
  • [ 94306-40-8 ]
  • [ 75954-35-7 ]
  • Phenyl 4-phenylthiobenzyl ether [ No CAS ]
Reference： [1]Russian Journal of Organic Chemistry,1997,vol. 33,p. 1601 - 1607
  • 12
  • [ 20600-22-0 ]
  • [ 139-66-2 ]
  • [ 94306-40-8 ]
  • [ 946-80-5 ]
  • [ 75954-35-7 ]
Reference： [1]Russian Journal of Organic Chemistry,1997,vol. 33,p. 1601 - 1607
  • 14
  • [ 930-69-8 ]
  • 4-bromo-benzyl halide [ No CAS ]
  • [ 75954-35-7 ]
Reference： [1]Journal of the Science of Food and Agriculture,1957,vol. 8,p. 566,567
  • 15
  • [ 28074-23-9 ]
  • p-brombenzylbis(dimethylglyoximato)pyridinecobalt(III) [ No CAS ]
  • [ 75954-35-7 ]
Reference： [1]Journal of the Chemical Society. Perkin transactions I,1980,p. 2021 - 2025
  • 16
  • [ 589-15-1 ]
  • [ 882-33-7 ]
  • [ 75954-35-7 ]
Reference： [1]Journal of Chemical Research,2006,p. 443 - 444
  • 17
  • [ 100375-00-6 ]
  • [ 75954-35-7 ]
Reference： [1]Chemistry Letters,2007,vol. 36,p. 1324 - 1325
[2]Synthesis,2008,p. 2543 - 2546
  • 18
  • [ 75954-35-7 ]
  • [ 100375-00-6 ]
  • [ 1122-91-4 ]
Reference： [1]Tetrahedron Letters,2008,vol. 49,p. 80 - 84
  • 19
  • [ 75954-35-7 ]
  • [ 88-10-8 ]
  • [ 1332344-50-9 ]
Reference： [1]Applied Organometallic Chemistry,2011,vol. 25,p. 669 - 674
  • 20
  • [ 75954-35-7 ]
  • [ 74-88-4 ]
  • [ 1332344-49-6 ]
Reference： [1]Applied Organometallic Chemistry,2011,vol. 25,p. 669 - 674
  • 21
  • [ 100-58-3 ]
  • sodium 4-bromobenzylsulfanesulfonate [ No CAS ]
  • [ 75954-35-7 ]
Reference： [1]Organic Letters,2014,vol. 16,p. 1196 - 1199
  • 22
  • [ 873-75-6 ]
  • [ 75954-35-7 ]
Reference： [1]Journal of Sulfur Chemistry,2014,vol. 35,p. 418 - 430
  • 23
  • [ 882-33-7 ]
  • 4-bromobenzyl diphenylphosphinite [ No CAS ]
  • [ 75954-35-7 ]
YieldReaction ConditionsOperation in experiment
In dichloromethane; at 20℃; for 12h;Inert atmosphere; General procedure: To a stirred solution of alcohol (1 mmol), Et3N (1.2 equiv.) in dry CH2Cl2 (1 mL) was successively added chlorodiphenylphosphine (1.2 equiv.) at RT under N2 atmosphere. After 2 h, benzothiazole-2-thiol (0.5 equiv.) and camphorquinone (1 equiv.) were added to the mixture, respectively. After the mixture was stirred for 12 h, it was extracted with CH2Cl2/H2O. The combined organic layers were washed with brine, dried over Na2SO4 and concentrated under reduced pressure. The residue was purified by preparative TLC on silica gel (hexane/EtOAc = 10/1) to afford the desired product.
Reference： [1]Journal of Sulfur Chemistry,2014,vol. 35,p. 418 - 430
  • 24
  • [ 589-17-3 ]
  • [ 36719-71-8 ]
  • [ 75954-35-7 ]
Reference： [1]Chemical Communications,2015,vol. 51,p. 941 - 944
  • 25
  • [ 62-53-3 ]
  • [ 75954-35-7 ]
Reference： [1]Chemical Communications,2015,vol. 51,p. 941 - 944
  • 26
  • [ 98-95-3 ]
  • [ 589-15-1 ]
  • [ 75954-35-7 ]
YieldReaction ConditionsOperation in experiment
89% With cobalt ferrite; potassium acetate; thiourea; In dimethyl sulfoxide; at 80℃; for 1.5h; A glass tube was charged with nitroarene (1 mmol), alkyl halide (1.2 mmol), thiourea (1.3 mmol), KOAc (1.5 mmol), DMSO (1 mL) and CoFe2O4 (5 mol%). The reaction mixture was stirred at 80 C for an appropriate amount of time. The progress of the reaction was monitored using TLC (n-hexane-EtOAc, 9:1). After completion of the reaction, the reaction mixture was allowed to cool to room temperature. The magnetic nanoparticles of the catalyst were collected using a magnet. Then, 10mL of water was added to the mixture and the product was extracted with ethyl acetate (3 × 10 mL). The organic phase was dried over CaCl2, concentrated under vacuum and purified by column chromatography on silica gel (n-hexane-EtOAc, 9:1). All products were known compounds and were identified by comparison of their 1H NMR spectra with those of authentic samples [25,26].
Reference： [1]Catalysis Communications,2017,vol. 94,p. 33 - 37
  • 27
  • [ 591-50-4 ]
  • [ 589-15-1 ]
  • [ 75954-35-7 ]
Reference： [1]Applied Organometallic Chemistry,2017,vol. 31
  • 28
  • [ 100-68-5 ]
  • [ 589-15-1 ]
  • [ 75954-35-7 ]
Reference： [1]Chemistry - An Asian Journal,2018,vol. 13,p. 3833 - 3837
  • 29
  • [ 75954-35-7 ]
  • [ 6011-14-9 ]
  • [ 5219-61-4 ]
Reference： [1]Chemical Communications,2019,vol. 55,p. 338 - 341
  • 30
  • [ 108-98-5 ]
  • [ 589-17-3 ]
  • [ 75954-35-7 ]
Reference： [1]Chemistry - A European Journal,2019,vol. 25,p. 6703 - 6706
  • 31
  • [ 75954-35-7 ]
  • [ 22979-35-7 ]
  • methyl 3-(4-bromophenyl)-2-phenyl-2-(phenylthio)propanoate [ No CAS ]
Reference： [1]Chemical Communications,2019,vol. 55,p. 8410 - 8413
[2]Chemistry - A European Journal,2019,vol. 25,p. 6703 - 6706

Tags: 75954-35-7; (4-Bromobenzyl)(phenyl)sulfane; Bromides

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