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[ CAS No. 76537-03-6 ] {[proInfo.proName]}

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Chemical Structure| 76537-03-6
Chemical Structure| 76537-03-6
Structure of 76537-03-6 * Storage: {[proInfo.prStorage]}
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Product Details of [ 76537-03-6 ]

CAS No. :76537-03-6 MDL No. :MFCD09931425
Formula : C5H2BrNOS Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 204.04 Pubchem ID :-
Synonyms :

Safety of [ 76537-03-6 ]

Signal Word:Danger Class:6.1
Precautionary Statements:P501-P261-P272-P270-P271-P264-P280-P284-P302+P352-P342+P311-P362+P364-P333+P313-P301+P310+P330-P304+P340+P311-P305+P351+P338+P310-P403+P233-P405 UN#:2206
Hazard Statements:H301+H331-H315-H318-H317-H334-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 76537-03-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 76537-03-6 ]

[ 76537-03-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 60-27-5 ]
  • [ 76537-03-6 ]
  • [ 7440-44-0 ]
  • [ 76537-04-7 ]
YieldReaction ConditionsOperation in experiment
In water; N,N-dimethyl-formamide; acetone; toluene; EXAMPLE XX 1-(5-Bromo-2-thienyl)-3-(tetrahydro-1-methyl-4-oxo-1H-imidazol-2-ylidene) urea To a stirred suspension of 3.0 g (26 mM) of <strong>[60-27-5]creatinine</strong> in 30 ml of anhydrous DMF was added a solution of 5.0 g (26.5 mM) of 5-bromo-2-thienyl isocyanate in 15 ml of toluene. The resulting mixture was heated at 75 C. for 3 hrs., cooled, and poured into 200 ml of water. The precipitate was collected, washed with ethanol and ether, and air-dried. The solid was dissolved in 250 ml hot acetone, treated with charcoal, filtered, and the filtrate diluted with water (250 ml). The resulting precipitate was collected, washed with acetone and then ether. Air-drying gave 2.3 g of the above urea as a buff powder, m.p. 192-193 C. (dec.). Anal. calcd. for C9 H9 BrN4 O2 S: C, 34.08; H, 2.86; N, 17.66. Found: C, 33.94; H, 3.04; N, 17.30.
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