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CAS No. : | 773-63-7 | MDL No. : | MFCD00614246 |
Formula : | C11H14N2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | N/A |
M.W : | 174.24 | Pubchem ID : | 594548 |
Synonyms : |
|
TPSA :Topological Polar Surface Area | 38.4 | H-Bond Acceptor Count : | 2 |
XLogP3 : | 1.6 | H-Bond Donor Count : | 1 |
SP3 : | 0.36 | Rotatable Bond Count : | 0 |
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
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Yield | Reaction Conditions | Operation in experiment |
---|---|---|
96% | Stage #1: With hydrogenchloride; tin(II) chloride dihdyrate In water for 2.00 h; Reflux Stage #2: With sodium hydrogencarbonate In water |
Example 2 5-amino-2,3,3-trimethyl-(3H)-indole (product B) A mixture of 6.6 g of product A, 43.7 g of stannous chloride dihydrate and 215 ml of hydrochloric acid is taken to reflux for two hours. After cooling down to ambient temperature and filtration, the solid collected is solubilized in 130 ml of water. This solution is neutralized by the addition of 20percent soda. The precipitate formed is filtered then washed with water and dried under vacuum in the presence of phosphoric anhydride. 5.4 g of product B is obtained (Yield: 96percent). |
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