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Chemical Structure| 77547-10-5 Chemical Structure| 77547-10-5

Structure of 77547-10-5

Chemical Structure| 77547-10-5

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Product Details of [ 77547-10-5 ]

CAS No. :77547-10-5
Formula : C11H13NO4S
M.W : 255.29
SMILES Code : O=CC1=CC=C(S(=O)(N2CCOCC2)=O)C=C1
MDL No. :MFCD11101102

Safety of [ 77547-10-5 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319
Precautionary Statements:P501-P270-P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330

Application In Synthesis of [ 77547-10-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 77547-10-5 ]

[ 77547-10-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 110-91-8 ]
  • [ 85822-16-8 ]
  • [ 77547-10-5 ]
YieldReaction ConditionsOperation in experiment
92% at 0 - 20℃; Morpholine (8.94 g, 102.62 mM; 2.1 eq.) was slowly dropped into a cooled (0 C.) solution of the 4-formylbenzene sulfonyl chloride (10.0 g, 48.87 mM; 1.0 eq.) and the mixture was slowly warmed to ambient temperature. TLC indicated complete disappearance of the starting sulfonyl chloride. The mixture was then poured on to ice-cold water, the solid was filtered, washed with water and vacuum dried to obtain the title sulfonamide as an off-white solid (11.5 g, 92%). The purity read 98% by LC/MS.
 

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