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CAS No. : | 79425-89-1 | MDL No. : | |
Formula : | C8H6N2S | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 162.21 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Class: | ||
Precautionary Statements: | UN#: | ||
Hazard Statements: | Packing Group: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With caesium carbonate; In N,N-dimethyl-formamide; at 60℃; for 2h; | General procedure: A mixture of 17 (257 mg, 1.1 mmol), ethyl1-bromocyclobutanecarboxylate (266 mg, 1.3 mmol) and Cs2CO3(371 mg, 1.1 mmol) in DMF was heated to 60 C and stirred for 2 hours. The mixture was cooled to room temperature and the resulting precipitate was filtered off. The collected filtrate was concentrated to give the ester ethyl1-((6-bromoquinolin-4-yl) thio)cyclobutanecarboxylate as an oil (300 mg, 77%). |