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[ CAS No. 79433-95-7 ] {[proInfo.proName]}

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Chemical Structure| 79433-95-7
Chemical Structure| 79433-95-7
Structure of 79433-95-7 * Storage: {[proInfo.prStorage]}
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Product Details of [ 79433-95-7 ]

CAS No. :79433-95-7 MDL No. :MFCD09954935
Formula : C14H17NO5 Boiling Point : -
Linear Structure Formula :- InChI Key :VVKAGQHUUDRPOI-NWDGAFQWSA-N
M.W : 279.29 Pubchem ID :688412
Synonyms :

Safety of [ 79433-95-7 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338 UN#:
Hazard Statements:H302-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 79433-95-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 79433-95-7 ]

[ 79433-95-7 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 155075-23-3 ]
  • [ 79433-95-7 ]
YieldReaction ConditionsOperation in experiment
23% With di-isopropyl azodicarboxylate; triphenylphosphine; 4-nitro-benzoic acid; In benzene; at 20℃; for 6h; To a stirred solution of the (2R, 4R)-I -benzyl 2-methyl 4-hydroxypyrrolidine-1,2-dicarboxylate (1.45 g, 5.2 mmol), triphenylphosphine (4.59 g, 17.5 mmol), and p- nitrobenzoic acid (2.6 g, 15.6 mmol) in dry benzene (10 ml) at room temperature was added diethylazodicarboxylate dropwise (2.57 ml, 17.5 mmol). The solution was then stirred at room temperature for 6 h, whereupon the volatile components were removed in vacuo and the residue purified by flash chromatography (silica gel, hexane-ethyl ether 1: 1, and again with hexane-ethyl ether-methylene chloride 2: 1 : 1). This residue was dissolved in methanol (10 ml), K2CO3 was added (0.02 g, 0.14 mmol) and the mixture was stirred for 1 h at room temperature. After removing the volatile components in vacuo, the residue was purified by flash chromatography (silica gel, gradient elution, using ethyl ether to ethyl acetate) to provide the title compound as a colorless oil (0.33 g, 23%).
  • 3
  • [ 79433-95-7 ]
  • [ 79775-07-8 ]
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