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Chemical Structure| 80604-68-8 Chemical Structure| 80604-68-8

Structure of 80604-68-8

Chemical Structure| 80604-68-8

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Product Details of [ 80604-68-8 ]

CAS No. :80604-68-8
Formula : C30H36O16
M.W : 652.60
SMILES Code : O=C1C=C(C2=CC=C(OC)C(OCCO)=C2)OC3=CC(O[C@H]4[C@@H]([C@H]([C@@H]([C@@H](CO[C@H]5[C@@H]([C@@H]([C@H]([C@H](C)O5)O)O)O)O4)O)O)O)=CC(O)=C13

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Application In Synthesis of [ 80604-68-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 80604-68-8 ]

[ 80604-68-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 520-27-4 ]
  • [ 107-07-3 ]
  • [ 80604-68-8 ]
YieldReaction ConditionsOperation in experiment
With triethylamine; In methanol; under 0.45 - 0.5 Torr;Large scale; The measurement of accurate 240.0kg methanol vacuum into the reactor, from the reactor mouth slowly added to the Austen Siming 60.0kg, triethylamine 1.0kg, the measurement of accurate 2-chloroethanol 22.5kg added to the reactor, open The autoclave heats the steam valve so that the pressure inside the kettle is kept at 0.45 ~ 0.50MPa for 1.0 ~ 3.0h. In the course of the reaction, the pressure is measured after the sampling test, otherwise the reaction continues until the qualified.Add 2.5 kg of activated charcoal to the decolorizer for 30 min.The bleach solution is filtered to the storage tank by hot pressing.From the storage tank to filter the good material to the crystallization tank on the crystallization of the cylinder, the water temperature is not higher than 30 , with concentrated hydrochloric acid to adjust the pH value of 3 to 4, crystallization 24 ~ 48h after centrifugation.
 

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