Home Cart Sign in  
Chemical Structure| 82301-30-2 Chemical Structure| 82301-30-2

Structure of 82301-30-2

Chemical Structure| 82301-30-2

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 82301-30-2 ]

CAS No. :82301-30-2
Formula : C9H7ClN2S2
M.W : 242.75
SMILES Code : ClC1=NC(SCC2=CC=CC=C2)=NS1

Safety of [ 82301-30-2 ]

Application In Synthesis of [ 82301-30-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 82301-30-2 ]

[ 82301-30-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 75-70-7 ]
  • [ 538-28-3 ]
  • [ 82301-30-2 ]
YieldReaction ConditionsOperation in experiment
With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In water; toluene; at 0℃; for 2h; To the mixture of 20 ml of toluene and 10 ml of water, 2.02 g of benzylisothiourea hydrochloride, 1.86 g of perchloromethylmercaptan and 46 mg of benzyltriethylammonium chloride were added, followed the solution of 1.6 g of sodium hydroxide dissolved to 10 ml of water was added dropwise at about 0 °C, and then stirred for 2 hours. Then, t-butylmethylether was added to the reaction mixture, and extracted. The organic layer was dried by anhydrous sodium salfate, and concentrated The residue obtaind was subjected to silica gel column chromatography (hexane:ethylacetate=20:1) to obtain 900 mg of 3-benzylthio-5-chloro-1,2,4-thiadiazole. 3-benzylthio-5-chloro-1,2,4-thiadiazole. 1H-NMR:7.60-7.20(m,5H)4.45(s,2H)
 

Historical Records