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Chemical Structure| 82418-39-1 Chemical Structure| 82418-39-1

Structure of 82418-39-1

Chemical Structure| 82418-39-1

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Product Details of [ 82418-39-1 ]

CAS No. :82418-39-1
Formula : C5H5N3
M.W : 107.11
SMILES Code : C#CCN1N=CN=C1
MDL No. :MFCD00607978

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Application In Synthesis of [ 82418-39-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 82418-39-1 ]

[ 82418-39-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 6086-21-1 ]
  • [ 106-96-7 ]
  • [ 82418-39-1 ]
YieldReaction ConditionsOperation in experiment
5.01 g Add 80 mmol of sodium n-butoxide to 50 mmol of 1,2,4-triazinium (compound) and 50 mlIn the mixture of n-butanol solution, the resulting suspension was stirred at 35 ° C for 50 min. Then add 70 mmol of bromopropyne at 80 °CThe condensation was refluxed for 16 h. The volatiles in the reaction mixture were removed in vacuo, washed with dichloromethane, and the solid impurities were filtered.After the solvent, a colorless liquid 1-propargyl-1,2,4-triazole 5.01 g was obtained.
 

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