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[ CAS No. 83277-30-9 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 83277-30-9
Chemical Structure| 83277-30-9
Structure of 83277-30-9 * Storage: {[proInfo.prStorage]}
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Product Details of [ 83277-30-9 ]

CAS No. :83277-30-9 MDL No. :
Formula : C7H13NO3 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W :159.18 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 83277-30-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 83277-30-9 ]

[ 83277-30-9 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 2604-39-9 ]
  • [ 83277-30-9 ]
  • [ 194732-40-6 ]
  • 2
  • [ 2789-25-5 ]
  • [ 83277-30-9 ]
  • [ 194732-21-3 ]
  • 3
  • [ 6452-57-9 ]
  • [ 616-38-6 ]
  • [ 83277-30-9 ]
YieldReaction ConditionsOperation in experiment
With sodium methylate In methanol Industry scale; 1.1 A reactor is charged with 392 kg of isopropylaminopropanediol, approximately 240 L of methanol, 6 to 7L of sodium methoxide (30%) and 270 L of dimethylcarbonate. The contents were heated up to allow reaction to occur. Solvent is removed by distillation.200 L water and ca 450 L of methylisobutylketone (MIBK) are then charged to the reactor. The reactor contents are then cooled down to <25°C. Tetrabutylammoniumhydrogensulphate (ca 2.5kg) and 520 kg of benzenesulphonylchloride are then added to the vessel under cooling. 30% sodium hydroxide is added to the reactorThe reactor contents are heated and phase separation performed, removing the aqueous layer. Solvent is distilled and the product oxazolidone sulphonate is isolated from methyl-tert-butylether (MTBE).Fig. 1 illustrates the infra red spectrum of oxazolidinone sulphate.Purity HPLC >98%
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