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Chemical Structure| 84827-59-8 Chemical Structure| 84827-59-8

Structure of 84827-59-8

Chemical Structure| 84827-59-8

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Product Details of [ 84827-59-8 ]

CAS No. :84827-59-8
Formula : C13H17NO2
M.W : 219.28
SMILES Code : O=C(OCC)CNC1CC2=C(C=CC=C2)C1

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Application In Synthesis of [ 84827-59-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 84827-59-8 ]

[ 84827-59-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 2338-18-3 ]
  • [ 105-36-2 ]
  • [ 84827-59-8 ]
YieldReaction ConditionsOperation in experiment
62% With triethylamine; In chloroform; acetonitrile; A. Ethyl N-(2-Indanyl) Glycinate 2-Aminoindan hydrochloride (50 g, 0.295 mol) was dissolved in acetonitrile (1 l) and triethylamine (65 g, 0.644 mol) was added. To the resulting solution was added dropwise ethyl bromoacetate (50 g, 0.297 mol) in acetonitrile (100 ml). The resulting mixture was stirred overnight at room temperature. Acetonitrile was evaporated and the residue was dissolved in chloroform. The chloroform was washed twice with water, dried over magnesium sulfate, filtered and evaporated to give the product as a tan oil (39.4 g, 62%) which was used in the next reaction without further purification. The product was characterized as its hydrochloride salt.
 

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