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Chemical Structure| 864528-04-1 Chemical Structure| 864528-04-1

Structure of 864528-04-1

Chemical Structure| 864528-04-1

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Product Details of [ 864528-04-1 ]

CAS No. :864528-04-1
Formula : C6H10N4O2
M.W : 170.17
SMILES Code : O=C(N1CCOCC1)CN=[N+]=[N-]
MDL No. :MFCD01320911

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Application In Synthesis of [ 864528-04-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 864528-04-1 ]

[ 864528-04-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 40299-87-4 ]
  • [ 864528-04-1 ]
YieldReaction ConditionsOperation in experiment
11% With sodium azide; In dimethyl sulfoxide; at 50℃; for 3h; General procedure: To a solution of bromide 3a-g (1.0 eq) in DMSO was added NaN3 (1.2 eq) at room temperature. Then the reaction mixture was heated to 50 C and kept for 3 h. Upon completion, EtOAc and H2O were added. The aqueous layer was extracted with EtOAc; the combined organic layers were washed with H2O for several times to remove the DMSO, and then washed with brine, dried over MgSO4 and evaporated to give the corresponding products 4a-g. Compounds 4d and 4e were known compounds [44] and therefore not characterized in this work.
 

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