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[ CAS No. 871332-67-1 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 871332-67-1
Chemical Structure| 871332-67-1
Structure of 871332-67-1 * Storage: {[proInfo.prStorage]}
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Product Details of [ 871332-67-1 ]

CAS No. :871332-67-1 MDL No. :MFCD07363796
Formula : C7H7BClNO3 Boiling Point : -
Linear Structure Formula :- InChI Key :PHYINASSDCHPRG-UHFFFAOYSA-N
M.W : 199.40 Pubchem ID :44886930
Synonyms :

Safety of [ 871332-67-1 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340+P312-P305+P351+P338-P332+P313-P337+P313-P362-P403+P233-P405-P501 UN#:
Hazard Statements:H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 871332-67-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 871332-67-1 ]

[ 871332-67-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 288-32-4 ]
  • [ 871332-67-1 ]
  • [ 1143020-40-9 ]
YieldReaction ConditionsOperation in experiment
39% In methanol at 65℃; for 18h; 41 Intermediate 41: 2-Chloro-5-(lH-imidazol-l-yl)benzamide; Copper(I) iodide (9.55 mg, 0.05 mmol) was added to 2-chloro-5-boronobenzamide (0.20 g, 1.00 mmol) and imidazole (82 mg, 1.20 mmol) in MeOH (4 mL) and the solution was heated at 65 0C for 18 hours. The reaction mixture was concentrated in vacuo and the residue was purified by chromatography on silica gel eluting with MeOH/DCM (0 - 10%) to give the title compound as a colourless solid (86 mg, 39%): 1H NMR 57.18 (IH, t), 7.68 - 7.71 (IH, m), 7.75 (IH, s), 7.77 - 7.81 (IH, m), 7.84 (IH, d), 7.88 (IH, t), 8.00 (IH, s), 8.39 (IH, s); MS 222.
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