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Chemical Structure| 875238-39-4 Chemical Structure| 875238-39-4

Structure of 875238-39-4

Chemical Structure| 875238-39-4

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Product Details of [ 875238-39-4 ]

CAS No. :875238-39-4
Formula : C7H10OS
M.W : 142.22
SMILES Code : OCC1=C(C)SC(C)=C1
MDL No. :MFCD11208334

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Application In Synthesis of [ 875238-39-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 875238-39-4 ]

[ 875238-39-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 26421-44-3 ]
  • [ 875238-39-4 ]
YieldReaction ConditionsOperation in experiment
800 mg With methanol; sodium tetrahydroborate; at 18 - 25℃; for 1h; To a stirred solution of 2,5-dimethylthiophene-3-carbaldehyde (1 g, 7.14 mmol) in MeOH (5 mL) at RT wasadded NaBH4 (542 mg, 14.28 mmol) in portions. After 1 h,a saturated ammonium chloride solution (1 0 mL) was addedto quench the reaction and extracted with EtOAc (20 mLx3).The combined organic phase was dried over Na2S04 andconcentrated. The residue was purified by silica-gel columnchromatography (Et0Ac/hexane=1:6) to give 800 mg of(2,5-dimethylthiophen-3-yl)methanol as a colorless oil. GCMS:142 (M+).
 

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