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Chemical Structure| 879093-13-7 Chemical Structure| 879093-13-7

Structure of 879093-13-7

Chemical Structure| 879093-13-7

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Product Details of [ 879093-13-7 ]

CAS No. :879093-13-7
Formula : C8H7ClO2
M.W : 170.59
SMILES Code : OC1C(Cl)=C2CCOC2=CC=1

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Application In Synthesis of [ 879093-13-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 879093-13-7 ]

[ 879093-13-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 40492-52-2 ]
  • [ 879093-13-7 ]
YieldReaction ConditionsOperation in experiment
With sulfuryl dichloride; In chloroform; at 0 - 20℃; 2,3-Dihydrobenzofuran-5-ol (400 mg, 2.94 mmol, 1.0 eq.) in CHCl3 (8 ml) was cooled to 0 0C and sulfuryl chloride (0.3 ml, 3.53 mmol, 1.2 eq.) in CHCl3 (25 ml) was added. The mixture was stirred overnight at ambient temperature. The reaction mixture was concentrated and the residue was purified by column chromatography (silica gel 100- 200 mesh, eluted with 15% EtOAc-hexane) to afford 4-chloro-2,3-dihydrobenzofuran-5- ol.
 

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