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[ CAS No. 89466-07-9 ]

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Chemical Structure| 89466-07-9
Chemical Structure| 89466-07-9
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Product Details of [ 89466-07-9 ]

CAS No. :89466-07-9 MDL No. :MFCD07437851
Formula : C6H7BN2O4 Boiling Point : 439.5°C at 760 mmHg
Linear Structure Formula :- InChI Key :N/A
M.W :181.94 g/mol Pubchem ID :-
Synonyms :

Safety of [ 89466-07-9 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P301+P312-P302+P352-P304+P340-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 89466-07-9 ]

  • Downstream synthetic route of [ 89466-07-9 ]

[ 89466-07-9 ] Synthesis Path-Downstream   1~20

  • 1
  • [ 99768-11-3 ]
  • [ 89466-07-9 ]
YieldReaction ConditionsOperation in experiment
With sulfuric acid
  • 2
  • [ 80500-27-2 ]
  • [ 89466-07-9 ]
  • 3
  • [ 80500-28-3 ]
  • [ 89466-07-9 ]
  • 5
  • [ 89466-07-9 ]
  • [ 1276122-65-6 ]
  • [ 1276122-43-0 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; sodium carbonate / 1,2-dimethoxyethane; water / 18 h / 90 °C / Inert atmosphere 2: hydrogenchloride; iron / ethanol; water / 4 h / 80 °C 3: triethylamine / dichloromethane / 2 h / 20 °C
  • 6
  • [ 89466-07-9 ]
  • C13H12F2N2O [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; sodium carbonate / 1,2-dimethoxyethane; water / 18 h / 90 °C / Inert atmosphere 2: hydrogenchloride; iron / ethanol; water / 4 h / 80 °C
  • 7
  • [ 89466-07-9 ]
  • [ 1221349-39-8 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; sodium carbonate / 1,2-dimethoxyethane; water / 18 h / 90 °C / Inert atmosphere 2.1: hydrogenchloride; iron / ethanol; water / 4 h / 80 °C 3.1: triethylamine / dichloromethane / 2 h / 20 °C 3.2: 3 h / 100 °C
  • 8
  • [ 89466-07-9 ]
  • [ 1259026-79-3 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 4 steps 1.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; sodium carbonate / 1,2-dimethoxyethane; water / 18 h / 90 °C / Inert atmosphere 2.1: hydrogenchloride; iron / ethanol; water / 4 h / 80 °C 3.1: triethylamine / dichloromethane / 2 h / 20 °C 3.2: 3 h / 100 °C 4.1: hydrogenchloride / diethyl ether; ethyl acetate
  • 9
  • [ 64248-56-2 ]
  • [ 89466-07-9 ]
  • [ 1259026-54-4 ]
YieldReaction ConditionsOperation in experiment
With sodium carbonate;tetrakis(triphenylphosphine) palladium(0); In 1,4-dioxane; water; at 110℃; for 1h;Microwave irradiation; To a mixture of 4-amino-2-nitrophenylboronic acid (606 mg, 3.30 mmol, 90%), 2-bromo-1,3-difluoro-benzene (579 mg, 3.00 mmol) and Pd(PPh3)4 (347 mg, 0.300 mmol) in 1,4-dioxane (9 mL) was added 2.0 M aqueous Na2CO3 (6.00 mL, 12.0 mmol). The resulting mixture was stirred at 110 C. under microwave irradiation for 1 h and then cooled to room temperature. The resulting mixture was treated with EtOAc (50 mL), then was washed with H2O and brine and was dried (Na2SO4). The solvent was removed under reduced pressure followed by flash chromatography of the residue on silica gel (5-40% EtOAc-hexanes) to yield a yellow solid. 1H-NMR (400 MHz, CDCl3) delta: 8.30 (s, 1H), 7.50 (dd, J=8.6, 1.8 Hz, 1H), 7.23-7.34 (m, 1H), 6.95-7.05 (m, 1H), 6.90 (d, J=8.6 Hz, 1H), 6.19 (br. s., 2H). Mass Spectrum (LCMS, ESI pos.) Calculated For C12H8F2N2O2: 251.1 (M+H), Measured: 251.0.
  • 10
  • [ 89466-07-9 ]
  • [ 1392517-54-2 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; water / 1 h / 110 °C / Microwave irradiation 2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 20 °C / Inert atmosphere 2.2: 2 h / 20 °C / Inert atmosphere
  • 11
  • [ 89466-07-9 ]
  • [ 1392517-56-4 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; water / 1 h / 110 °C / Microwave irradiation 2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 20 °C / Inert atmosphere 2.2: 2 h / 20 °C / Inert atmosphere 3.1: acetic acid; iron / ethanol / 1 h / 110 °C / Microwave irradiation
  • 12
  • 4-[(4-chloro-6-phenylpyrimidin-2-ylamino)methyl]cyclohexanecarboxylic acid ethyl ester [ No CAS ]
  • [ 89466-07-9 ]
  • C26H29N5O4 [ No CAS ]
YieldReaction ConditionsOperation in experiment
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate In 1,4-dioxane; water at 100℃; for 1h; Microwave irradiation; Sealed tube;
  • 13
  • [ 89466-07-9 ]
  • 4-(1-methyl-1H-pyrazol-4-yl)benzene-1,2-diamine [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; potassium carbonate / propan-1-ol / 1 h / 120 °C 2: palladium 10% on activated carbon; hydrogen / dichloromethane; ethanol / 72 h / 20 °C
  • 14
  • [ 89466-07-9 ]
  • tert-butyl 4-[(2-[6-(1-methyl-1H-pyrazol-4-yl)-1H-benzimidazol-2-yl]amino}pyridin-4-yl)methyl]piperazine-1-carboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1.1: bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; potassium carbonate / propan-1-ol / 1 h / 120 °C 2.1: palladium 10% on activated carbon; hydrogen / dichloromethane; ethanol / 72 h / 20 °C 3.1: 1H-imidazole / dichloromethane / 0 - 20 °C 3.2: 2 h / 20 °C 3.3: 20 °C
  • 15
  • [ 89466-07-9 ]
  • 4-(4-amino-3-nitrophenyl)pyrimidin-5-ol [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; potassium carbonate / propan-1-ol / 3 h / Reflux 2: sodium thiomethoxide / N,N-dimethyl-formamide / 3 h / 60 °C
  • 16
  • [ 89466-07-9 ]
  • 2-nitro-4-{5-[(propan-2-yl)oxy]pyrimidin-4-yl}aniline [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; potassium carbonate / propan-1-ol / 3 h / Reflux 2: sodium thiomethoxide / N,N-dimethyl-formamide / 3 h / 60 °C 3: potassium carbonate / N,N-dimethyl acetamide / 1 h / 70 °C
  • 17
  • [ 89466-07-9 ]
  • 4-{5-[(propan-2-yl)oxy]pyrimidin-4-yl}benzene-1,2-diamine [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 4 steps 1: bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; potassium carbonate / propan-1-ol / 3 h / Reflux 2: sodium thiomethoxide / N,N-dimethyl-formamide / 3 h / 60 °C 3: potassium carbonate / N,N-dimethyl acetamide / 1 h / 70 °C 4: palladium 10% on activated carbon; hydrogen / dichloromethane; ethanol / 2 h / 20 °C
  • 18
  • [ 89466-07-9 ]
  • tert-butyl 4-[(1R)-1-{2-[(6-{5-[(propan-2-yl)oxy]pyrimidin-4-yl}-1H-benzimidazol-2-yl)amino]pyridin-4-yl}ethyl]piperazine-1-carboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 5 steps 1.1: bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; potassium carbonate / propan-1-ol / 3 h / Reflux 2.1: sodium thiomethoxide / N,N-dimethyl-formamide / 3 h / 60 °C 3.1: potassium carbonate / N,N-dimethyl acetamide / 1 h / 70 °C 4.1: palladium 10% on activated carbon; hydrogen / dichloromethane; ethanol / 2 h / 20 °C 5.1: 1H-imidazole / dichloromethane / 0 - 20 °C 5.2: 2 h / 20 °C 5.3: 20 °C
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