Alternatived Products of [ 911102-04-0 ]
Product Details of [ 911102-04-0 ]
CAS No. : | 911102-04-0 |
MDL No. : | MFCD31381636 |
Formula : |
C15H24N2O8
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Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
360.36
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Pubchem ID : | - |
Synonyms : |
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Safety of [ 911102-04-0 ]
Signal Word: | |
Class: | |
Precautionary Statements: | |
UN#: | |
Hazard Statements: | |
Packing Group: | |
Application In Synthesis of [ 911102-04-0 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 911102-04-0 ]
- 1
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[ 911102-04-0 ]
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[ 134978-97-5 ]
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[ 1069067-08-8 ]
Yield | Reaction Conditions | Operation in experiment |
86% |
With sodium hydrogencarbonate; In tetrahydrofuran; water; for 4h; |
H-AEEA-OH (9.8 g, 60 mmol) and NaHCO3 (8.4 g, 100 mmol) were dissolved in 100 ml deionized water, a solution of Boc-AEEA-OSu (18.0 g, 50 mmol) dissolved in THF (100 ml) was added while stirring, and after the dropwise addition was completed, the reaction was continued for 4 h. TLC showed that the reaction of Boc-AEEA-OSu had almost completed. Vacuum concentration was performed to remove the organic solvent, the aqueous phase was washed with EA (100 ml*3), the pH of the aqueous phase was adjusted to 3 with 1N HCl, and extraction was performed with EA (100 ml*2). After that, the organic phases were combined, washing was performed with saturated salt water (100 ml*3), drying was performed with anhydrous sodium sulfate, and vacuum concentration was performed to obtain 17.6 g of Boc-AEEA-AEEA-OH with yield: 86%, purity: 95.8%, MS: 409.4 (M+1). |