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[ CAS No. 912762-85-7 ] {[proInfo.proName]}

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Chemical Structure| 912762-85-7
Chemical Structure| 912762-85-7
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Product Details of [ 912762-85-7 ]

CAS No. :912762-85-7 MDL No. :MFCD08692522
Formula : C14H22N2O3 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 266.34 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 912762-85-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 912762-85-7 ]

[ 912762-85-7 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 912762-85-7 ]
  • [ 64507-38-6 ]
  • C24H26BrN3O4 [ No CAS ]
YieldReaction ConditionsOperation in experiment
With N-ethyl-N,N-diisopropylamine; HATU In tetrahydrofuran at 14℃; for 16h; 34.2 Step 2 Compound 34b (800 mg, 3.17 mmol) was dissolved in tetrahydrofuran (10 mL), and then O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate (1.27 g, 3.33 mmol), N,N-diisopropylethylamine (1.23 g, 9.52 mmol, 1.66 mL) and compound 33d (535 mg, 1.98 mmol) were added thereto, the reaction mixture was stirred at 14 °C for 16 hours After the completion of the reaction, the reaction mixture was concentrated under reduced pressure. The residue was purified by thin layer chromatography to give compound 34c.
  • 2
  • [ 912762-85-7 ]
  • [ 125096-73-3 ]
  • [ 2771136-45-7 ]
YieldReaction ConditionsOperation in experiment
With anhydrous sodium carbonate In isopropanol at 60℃; for 15h; 6.4 the fourth step Compound 6-4 (220 mg, 757 μmol) and Intermediate B (205 mg, 757 μmol) were dissolved in isopropanol (5 mL) and sodium carbonate (161 mg, 1.51 mmol) was added.The reaction solution was stirred at 60 degrees Celsius for 15 hours.The reaction solution was concentrated under reduced pressure, and the obtained crude product was separated and purified by column chromatography (eluent: petroleum ether/ethyl acetate, 10/14/1, V/V) to obtain compound 6-5.
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