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Chemical Structure| 913737-84-5 Chemical Structure| 913737-84-5

Structure of 913737-84-5

Chemical Structure| 913737-84-5

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Product Details of [ 913737-84-5 ]

CAS No. :913737-84-5
Formula : C36H22N2O
M.W : 498.57
SMILES Code : C12=CC=C(N3C4=C(C5=C3C=CC=C5)C=CC=C4)C=C1C6=CC(N7C8=C(C9=C7C=CC=C9)C=CC=C8)=CC=C6O2

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Application In Synthesis of [ 913737-84-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 913737-84-5 ]

[ 913737-84-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 10016-52-1 ]
  • [ 86-74-8 ]
  • [ 913737-84-5 ]
YieldReaction ConditionsOperation in experiment
85% With N,N-dimethyl acetamide; copper; potassium carbonate; at 130℃; for 24h;Inert atmosphere; Under a nitrogen atmosphere, <strong>[10016-52-1]2,8-dibromodibenzofuran</strong> (1.0 mole), carbazole (2.0 moles), copper powder (3.0 moles), potassium carbonate (1.5 moles) were mixed in 300 ml of DMAc (dimethylacetamide) and stirred at 130° C. for 24 hours. Afier the resulting reaction liquid was cooled to room temperature, 1 L of toluene was added to the liquid. The mixture was washed three times with distilled water, and the solvent was removed from the washed product by distillation under a reduced pressure atmosphere. The residue was purified by silica gel flash chromatography (n-heptane:toluene=4: 1 to 3:1) to give intermediate 1 with a yield of 85percent.
 

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