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Chemical Structure| 924909-11-5 Chemical Structure| 924909-11-5

Structure of 924909-11-5

Chemical Structure| 924909-11-5

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Product Details of [ 924909-11-5 ]

CAS No. :924909-11-5
Formula : C6H5N3O
M.W : 135.12
SMILES Code : [O-][N+]1=CC=CC2=C1NN=C2
MDL No. :MFCD13175992

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Application In Synthesis of [ 924909-11-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 924909-11-5 ]

[ 924909-11-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 271-73-8 ]
  • [ 924909-11-5 ]
YieldReaction ConditionsOperation in experiment
47.3 g With 3-chloro-benzenecarboperoxoic acid; In 1-methyl-pyrrolidin-2-one; at 20℃; for 1h; To a solution of lH-pyrazolo[3,4-Z?]pyridine (50 g, 0.42 mol) in NMP (300 mL) was added a solution of m-CPBA (84 g, 0.49 mol) in NMP (200 mL) dropwise. After being stirred at room temperature for lhr, the reaction mixture was diluted with tert-butyl methyl ether (600 mL) and stirred vigorously for 30 min. The precipitate was collected by filtration and washed with MTBE to afford 1H- pyrazolo[3,4-Z?]pyridine 7-oxide (47.3 g) as a off-white solid.LC-MS (ESI): mlz, (Mu+Eta) + , 136.0.
 

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