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CAS No. : | 928642-02-8 | MDL No. : | N/A |
Formula : | C27H24Br3N | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 602.20 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Warning | Class: | |
Precautionary Statements: | P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313 | UN#: | |
Hazard Statements: | H315-H319 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
10.4 g | With tetrakis(triphenylphosphine) palladium(0); dipotassium hydrogen phosphate; In 1,4-dioxane; water; at 80℃; for 7h; | 1. 3g (1. 17 millimols) of Pd (PPh 3) 4 is, 200 ml of water and 200 ml of benzodioxane 6. 2g (10. 4 millimols) of 4, 4, 8, 8, 12, 12-hexamethylindane -2, 6, 10-tribromostyrene -4H, 8H, 12H-dihydrobenzo [1, 9] [...] [3, 4, 5, 6, 7-defg] Aminoacridine (from the example 1) and 9. 9g (31. 2 millimols) of 10-(1-naphthyl)-9-dimethylanthryl arylboronic acid, 14. 9g (70. 2 millimols) of K 3 PO 4 unsatd. added to a mixture of nitrogen, 7 80 C heated in suspension. 0. 08g of NaCN is, then added, the water phase is separated. The organic phase is water, is 2 , Na 2 SO 4 the drying. The residue is obtained, the recrystallization from toluene. The precipitated crystals, the suction filtration, washed in 50 ml ethanol vacuum dried, 99 by HPLC. 6% purity of> 10. 4g (8. 1 millimols) (corresponding to 80% of a theoretical value) of the product is obtained. |