[ CAS No. 929-77-1 ]

Name: 929-77-1|Methyl docosanoate|98%
Brand: Ambeed
SKU: A694195
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{[proInfo.proName]} (Synonyms:Methyl behenate) ,{[proInfo.pro_purity]}

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Quality Control of [ 929-77-1 ]

COA NMR CNMR HPLC LC-MS

Related Doc. of [ 929-77-1 ]

SDS Specification

Alternatived Products of [ 929-77-1 ]

Product Details of [ 929-77-1 ]

CAS No. :	929-77-1	MDL No. :	MFCD00009347
Formula :	C₂₃H₄₆O₂	Boiling Point :	-
Linear Structure Formula :	-	InChI Key :	QSQLTHHMFHEFIY-UHFFFAOYSA-N
M.W :	354.61	Pubchem ID :	13584
Synonyms :	Methyl behenate

Safety of [ 929-77-1 ]

Signal Word:	Warning	Class:	N/A
Precautionary Statements:	P261-P301+P312-P302+P352-P304+P340-P305+P351+P338	UN#:	N/A
Hazard Statements:	H302-H315-H319-H335	Packing Group:	N/A
GHS Pictogram:

Application In Synthesis of [ 929-77-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Upstream synthesis route of [ 929-77-1 ]
Downstream synthetic route of [ 929-77-1 ]

[ 929-77-1 ] Synthesis Path-Upstream 1~4

1
[ 67-56-1 ]
[ 8001-22-7 ]
[ 14663-11-7 ]
[ 88400-02-6 ]
[ 10030-74-7 ]
[ 112-62-9 ]
[ 112-63-0 ]
[ 1120-34-9 ]
[ 2733-88-2 ]
[ 124-10-7 ]
[ 112-39-0 ]
[ 1731-92-6 ]
[ 112-61-8 ]
[ 1120-28-1 ]
[ 929-77-1 ]
[ 2442-49-1 ]
[ 10305-59-6 ]
[ 37929-05-8 ]
[ 56-81-5 ]

Reference： [1] Patent: WO2007/12190, 2007, A1, . Location in patent: Page/Page column 16-18

2
[ 67-56-1 ]
[ 14663-11-7 ]
[ 88400-02-6 ]
[ 10030-74-7 ]
[ 112-62-9 ]
[ 112-63-0 ]
[ 1120-34-9 ]
[ 2733-88-2 ]
[ 124-10-7 ]
[ 112-39-0 ]
[ 1731-92-6 ]
[ 112-61-8 ]
[ 1120-28-1 ]
[ 929-77-1 ]
[ 2442-49-1 ]
[ 10305-59-6 ]
[ 37929-05-8 ]
[ 56-81-5 ]

Reference： [1] Patent: WO2007/12190, 2007, A1, . Location in patent: Page/Page column 13-15

3
[ 67-56-1 ]
[ 14663-11-7 ]
[ 88400-02-6 ]
[ 10030-74-7 ]
[ 112-62-9 ]
[ 112-63-0 ]
[ 1120-34-9 ]
[ 2733-88-2 ]
[ 124-10-7 ]
[ 112-39-0 ]
[ 1731-92-6 ]
[ 112-61-8 ]
[ 1120-28-1 ]
[ 929-77-1 ]
[ 2442-49-1 ]
[ 10305-59-6 ]
[ 37929-05-8 ]
[ 56-81-5 ]

Reference： [1] Patent: WO2007/12190, 2007, A1, . Location in patent: Page/Page column 10-12

4
[ 929-77-1 ]
[ 661-19-8 ]

Reference： [1] Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1996, vol. 35, # 12, p. 1239 - 1241
[2] Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2002, vol. 41, # 8, p. 1724 - 1726

[ 929-77-1 ] Synthesis Path-Downstream 1~51

1
[ 908094-01-9 ]
[ 112-85-6 ]
[ 929-77-1 ]

Yield	Reaction Conditions	Operation in experiment
	With diethyl ether
	In Petroleum ether Acidic conditions;

Reference： [1]Dryden; Welsh [Australian Journal of Scientific Research, Series A: Physical Sciences, 1951, vol. 4, p. 616,619,623]
[2]Location in patent: body text Korobko; Turko; Shokun; Chernyak; Pokrovskii; Smetankina; Kerimzhanova; Baltaev [Chemistry of Natural Compounds, 2008, vol. 44, # 3, p. 359 - 360]

2
[ 67-56-1 ]
[ 112-85-6 ]
[ 929-77-1 ]

Yield	Reaction Conditions	Operation in experiment
	With sulfuric acid
	With sulfuric acid for 7h; Heating;
	With sulfuric acid Heating;

Reference： [1]Levene; Taylor [Journal of Biological Chemistry, 1924, vol. 59, p. 921]
[2]Deshmukh; Veeresh [Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1996, vol. 35, # 12, p. 1239 - 1241]
[3]Yildirim, Ayhan [Acta Chimica Slovenica, 2015, vol. 62, # 2, p. 473 - 478]

3
[ 56630-69-4 ]
[ 929-77-1 ]

Yield	Reaction Conditions	Operation in experiment
	With hydrogen; nickel at 190 - 200℃; Hydrogenation;

Reference： [1]McGregor; Beal [Journal of the American Chemical Society, 1926, vol. 48, p. 3153]

4
[ 929-77-1 ]
[ 112-85-6 ]

Yield	Reaction Conditions	Operation in experiment
	With potassium hydroxide

Reference： [1]Joshi, U. R.; Kapadi, A. H. [Synthetic Communications, 1984, vol. 14, # 7, p. 681 - 686]

5
[ 818-88-2 ]
[ 544-63-8 ]
[ 929-77-1 ]

Yield	Reaction Conditions	Operation in experiment
45.2%	With sodium methylate In methanol at 35℃; electrolysis on Pt electrode, 0.05 amps, 50-60 volts;

Reference： [1]Joshi, U. R.; Kapadi, A. H. [Synthetic Communications, 1984, vol. 14, # 7, p. 681 - 686]

6
oceanapin E [ No CAS ]
[ 929-77-1 ]
(4E)-2-amino-16-methyloctadec-4-ene-1,3-diol [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
	With methanol; sulfuric acid for 6h; Heating;

Reference： [1]Mancini; Guella; Debitus; Pietra [Helvetica Chimica Acta, 1994, vol. 77, # 1, p. 51 - 58]

7
methyl erucate [ No CAS ]
[ 929-77-1 ]

Yield	Reaction Conditions	Operation in experiment
98%	With hydrogen In dichloromethane at 20℃;

Reference： [1]Villemin, Didier; Letulle, Marguerite [Synthetic Communications, 1989, vol. 19, # 16, p. 2833 - 2840]

8
[ 67-56-1 ]
C₅₅H₁₁₁N₂O₁₁P [ No CAS ]
[ 929-77-1 ]
sphinganine (d22:0) [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
	With hydrogenchloride at 90℃; for 2h;

Reference： [1]Noda; Tanaka; Tsujino; Miura; Miyahara; Hayakawa [Chemical and Pharmaceutical Bulletin, 1995, vol. 43, # 4, p. 567 - 570]

9
[ 67-56-1 ]
N-docosanoyl-1-O-<6-O-(2-trimethylammonioethoxy)phosphinate-β-D-galactopyranosyl>-(4E,8Z,11Z)-docosaspingatrienine [ No CAS ]
[ 929-77-1 ]

Yield	Reaction Conditions	Operation in experiment
	With hydrogenchloride at 90℃; for 1h;

Reference： [1]Noda; Tanaka; Tsujino; Miura; Miyahara; Hayakawa [Chemical and Pharmaceutical Bulletin, 1995, vol. 43, # 4, p. 567 - 570]

10
[ 929-77-1 ]
[ 661-19-8 ]

Yield	Reaction Conditions	Operation in experiment
	With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃; for 3h;
	With lithium aluminium tetrahydride In tetrahydrofuran

Reference： [1]Deshmukh; Veeresh [Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1996, vol. 35, # 12, p. 1239 - 1241]
[2]Yadav, Ashok K.; Singh, Arpita [Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2002, vol. 41, # 8, p. 1724 - 1726]

11
Docosanoic acid ((E)-(1S,2R)-2-hydroxy-1-hydroxymethyl-15-methyl-hexadec-3-enyl)-amide [ No CAS ]
[ 929-77-1 ]
(E)-(2S,3R)-2-Amino-16-methyl-heptadec-4-ene-1,3-diol [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
0.7 mg	With hydrogenchloride; methanol at 76℃; for 18h;

Reference： [1]Hattori; Adachi; Shizuri [Journal of Natural Products, 1998, vol. 61, # 6, p. 823 - 826]

12
[ 67-56-1 ]
[ 27888-44-4 ]
[ 929-77-1 ]

Yield	Reaction Conditions	Operation in experiment
	With sulfuric acid In water for 4h; Heating;

Reference： [1]Agrawal, Shalini; Garg [Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1997, vol. 36, # 4, p. 343 - 346]

13
[ 929-77-1 ]
[ 120747-17-3 ]

Yield	Reaction Conditions	Operation in experiment
	With diethyl ether