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CAS No. : | 938080-25-2 | MDL No. : | MFCD11504945 |
Formula : | C13H17BO2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | HNJLVOQORSGCLB-UHFFFAOYSA-N |
M.W : | 216.08 | Pubchem ID : | 46739137 |
Synonyms : |
|
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P330-P363-P501 | UN#: | |
Hazard Statements: | H302-H312-H332 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
75% | Stage #1: 5,5-dimethyl-2-(1-phenylethen-1-yl)-1,3,2-dioxaborinane; carbon dioxide With [Ni(N,N'-bis[2,6-bis(diphenylmethyl)-4-methylphenyl]imidazole-2-ylidene)(allyl)Cl]; potassium <i>tert</i>-butylate In toluene at 100℃; for 15h; Schlenk technique; Inert atmosphere; Stage #2: With hydrogenchloride In water; ethyl acetate; toluene at 20℃; | |
60% | Stage #1: 5,5-dimethyl-2-(1-phenylethen-1-yl)-1,3,2-dioxaborinane; carbon dioxide With copper(l) iodide; cesium fluoride In N,N-dimethyl-formamide at 90℃; for 10h; Stage #2: With hydrogenchloride; water In N,N-dimethyl-formamide |
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