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CAS No. : | 94009-16-2 | MDL No. : | MFCD02665237 |
Formula : | C11H10N2O2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 202.21 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Class: | ||
Precautionary Statements: | UN#: | ||
Hazard Statements: | Packing Group: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
63% | In acetic acid at 120 - 130℃; for 0.5h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With hydrogen In ethanol |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 4 steps 1: hydrogen / 10percent Pd/C / ethanol 2: ethanol / 0.5 h / 120 °C 3: 53.8 percent / diphenyl ether / 0.5 h / Heating 4: 52.8 percent / 10percent NaOH / ethanol; H2O / 1 h / Heating |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 7 steps 1: hydrogen / 10percent Pd/C / ethanol 2: ethanol / 0.5 h / 120 °C 3: 53.8 percent / diphenyl ether / 0.5 h / Heating 4: 52.8 percent / 10percent NaOH / ethanol; H2O / 1 h / Heating 5: 55 percent / potassium carbonate / dimethylformamide / 4 h / 80 °C 6: 71.3 percent / 10percent NaOH / H2O; ethanol / 0.5 h / Heating 7: 43 percent / hydrogen / 5percent Rh/Al2O3 / acetic acid / 7 h / 50 °C / 3040 Torr |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 3 steps 1: hydrogen / 10percent Pd/C / ethanol 2: ethanol / 0.5 h / 120 °C 3: 53.8 percent / diphenyl ether / 0.5 h / Heating |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 6 steps 1: hydrogen / 10percent Pd/C / ethanol 2: ethanol / 0.5 h / 120 °C 3: 53.8 percent / diphenyl ether / 0.5 h / Heating 4: 52.8 percent / 10percent NaOH / ethanol; H2O / 1 h / Heating 5: 55 percent / potassium carbonate / dimethylformamide / 4 h / 80 °C 6: 71.3 percent / 10percent NaOH / H2O; ethanol / 0.5 h / Heating |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 5 steps 1: hydrogen / 10percent Pd/C / ethanol 2: ethanol / 0.5 h / 120 °C 3: 53.8 percent / diphenyl ether / 0.5 h / Heating 4: 52.8 percent / 10percent NaOH / ethanol; H2O / 1 h / Heating 5: 55 percent / potassium carbonate / dimethylformamide / 4 h / 80 °C |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: hydrogen / 10percent Pd/C / ethanol 2: ethanol / 0.5 h / 120 °C |