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Chemical Structure| 944893-74-7 Chemical Structure| 944893-74-7

Structure of 944893-74-7

Chemical Structure| 944893-74-7

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Product Details of [ 944893-74-7 ]

CAS No. :944893-74-7
Formula : C11H11NO
M.W : 173.21
SMILES Code : O=CC1=CC2=C(N(CC)C=C2)C=C1
MDL No. :MFCD09455244
InChI Key :WWOYPVXWHICMOY-UHFFFAOYSA-N
Pubchem ID :17221160

Safety of [ 944893-74-7 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H317-H319
Precautionary Statements:P280-P305+P351+P338

Application In Synthesis of [ 944893-74-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 944893-74-7 ]

[ 944893-74-7 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 944893-74-7 ]
  • [ 2840-44-0 ]
  • C21H18FNO [ No CAS ]
  • 2
  • [ 944893-74-7 ]
  • [ 2840-44-0 ]
  • (2E)-2-[(1-ethyl-1H-indol-5-yl)methylidene]-7-fluoro-1,2,3,4-tetrahydronaphthalen-1-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
With sodium hydroxide; In ethanol; at 20℃; Sodium hydroxide (8 M, 0.6 mL) was added to a mixture of <strong>[2840-44-0]7-fluoro-1-tetralone</strong> (82 mg, 0.5 mmol) and N-ethyl-indole-5-carbaldehyde (85 mg, 0.5 mmol) in three (3) mL of EtOH and stirred at room temperature overnight. The resulting precipitate was collected via filtration, and washed with EtOH and water to yield Compound 8 as a fineyellow solid.?H NMR (400MHz, DMSO-d6): 1.37(t,J= 6.4 Hz, 3H), 2.91-2.95 (m, 2H),2.91-2.95 (m, 2H), 4.24 (q, J= 6.4 Hz, 2H), 6.52 (d, J= 3.2 Hz, 1H), 7.35 (d, J= 8.4,1.6 Hz, 1H), 7.37 (m, 3H), 7.56-7.58 (d, J 8.4 Hz, 1H), 7.63 (d, J 8.8, 2.4 Hz, 1H),7.82 (s, 1H), 7.95 (s, 1H). ESI(+)- MS m/z calc?d for C2,H,8FNO: 319.38; found: 321.3(M+2H), 640.8 (2M+2H)2.
 

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