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Chemical Structure| 948552-24-7 Chemical Structure| 948552-24-7

Structure of 948552-24-7

Chemical Structure| 948552-24-7

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Product Details of [ 948552-24-7 ]

CAS No. :948552-24-7
Formula : C56H40N2
M.W : 740.93
SMILES Code : C1(C2=CC=C(C3=CC=C(C4=CC=C(N(C5=C6C=CC=CC6=CC=C5)C7=CC=CC=C7)C=C4)C=C3)C=C2)=CC=C(N(C8=C9C=CC=CC9=CC=C8)C%10=CC=CC=C%10)C=C1
MDL No. :MFCD09833571

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Application In Synthesis of [ 948552-24-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 948552-24-7 ]

[ 948552-24-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 352359-42-3 ]
  • [ 948552-24-7 ]
YieldReaction ConditionsOperation in experiment
25% With [2,2]bipyridinyl; triphenylphosphine; sodium bromide; nickel(I) bromide; zinc; In N,N-dimethyl-formamide; at 70℃; for 2h;Inert atmosphere; 63.9 g of 4-(Ν-1-naphthalene-N-phenyl)-amine in 0.8 M anhydrous dimethylformamide in a 2.5 M sulfonation degree vial and argon atmosphere Butyl-4'-bromobiphenyl was added dropwise to a solution of 130 g of zinc, 16.8 g of sodium bromide, 13 g of triphenylphosphine, 12 g of nickel bromide, 6 g of 2, Of anhydrous dimethylformamide while stirring at 70 C. The mixture was stirred at 70 C for an additional 2 hours. The stock is sucked from the zinc by suction. The solution was concentrated in a rotary evaporator, reacted with 2 L methanol, and the product of Shen Dian was sucked away by suction. Wash this with 0.2 L of methanol. The remaining material was grown in 0.5 L acetic acid at 10. <3 agitated, and sucked by suction after cooling. This step was repeated with L acetic acid and then rinsed with 0.1 L acetic acid and 0.03 L acetone. In each example, the product was heated to reflux with 0.36 L of toluene and sucked by suction after cooling. And then dried in a drying oven at 70 C
 

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