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Chemical Structure| 951322-70-6 Chemical Structure| 951322-70-6

Structure of 951322-70-6

Chemical Structure| 951322-70-6

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Product Details of [ 951322-70-6 ]

CAS No. :951322-70-6
Formula : C22H22N2
M.W : 314.42
SMILES Code : N[C@H](C1=CC=CC=C1)[C@@H](C2=CC=CC=C2)N3CC4=C(C=CC=C4)C3

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Application In Synthesis of [ 951322-70-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 951322-70-6 ]

[ 951322-70-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 2631-77-8 ]
  • [ 951322-70-6 ]
  • 4,6-diiodo-2-{(trans-2-(isoindolin-2-yl)-1,2-diphenylethylimino)methyl}phenol [ No CAS ]
YieldReaction ConditionsOperation in experiment
70% In ethanol; at 20℃;Inert atmosphere; Schlenk technique; Molecular sieve; General procedure: To a mixture of salicylaldehyde 1a-f, 1,3-dihydro-α,β-diphenyl-2H-isoindole -2-ethanamine 2 (equivalent to 1a-f), and several 4 Å sieves in a septum capped Schlenk tube was added anhydrous ethanol (ca. 10 mL per mmol of 1a-f) via syringe at 20 C with stirring under nitrogen. After stirring the resulting mixture overnight, the solvent was removed under vacuum, and the residue was purified by flash chromatography on silica gel (Vethyl acetate/Vpetroleum ether = 1/20) to give the brown target ligands 3a-f.
 

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