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Chemical Structure| 954417-62-0 Chemical Structure| 954417-62-0

Structure of 954417-62-0

Chemical Structure| 954417-62-0

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Product Details of [ 954417-62-0 ]

CAS No. :954417-62-0
Formula : C9H9F3N2O
M.W : 218.18
SMILES Code : O=C(NC)C1=CC=C(N)C(C(F)(F)F)=C1

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Application In Synthesis of [ 954417-62-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 954417-62-0 ]

[ 954417-62-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 887144-94-7 ]
  • [ 6274-22-2 ]
  • [ 954417-62-0 ]
YieldReaction ConditionsOperation in experiment
85% With tris[2-phenylpyridinato-C2,N]iridium(III); In N,N-dimethyl-formamide; at 20℃;Inert atmosphere; Irradiation; Under nitrogen or argon, 0.4 mmol, 0.2mmol, Ir(ppy) 3(2mg) and DMF1 ml was added to the reaction flask, followed by blue LED lights(7W) at room temperature irradiation straight trivalent iodine reagent completeconversion of the reaction. Add 10 ml of saturated Na 2CO 3Aqueous solution, andextracted three times with ethyl acetate, the organic layer was washed with water andonce with saturated brine, dried over anhydrous Na 2SO 4The organic layer was dried.Column chromatography (eluent: petroleum ether 60-90: ethyl acetate = 10: 1-3: 1) to give the product in 85% yield.
 

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