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Chemical Structure| 960403-88-7 Chemical Structure| 960403-88-7

Structure of 960403-88-7

Chemical Structure| 960403-88-7

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Product Details of [ 960403-88-7 ]

CAS No. :960403-88-7
Formula : C13H18N2O
M.W : 218.30
SMILES Code : CC(C1N(C)CCNC1C2=CC=CC=C2)=O

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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 960403-88-7 ]

[ 960403-88-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 108-24-7 ]
  • [ 5271-27-2 ]
  • [ 960403-88-7 ]
YieldReaction ConditionsOperation in experiment
94% With triethylamine; In dichloromethane; water; 1 -Methyl-3-phenylpiperazine (17.6 g; 0.1 mol) was dissolved in 100 dichloromethane. Acetic anhydride and triethylamine were added. Aqueous work-up yielded >100 percent of smelly oil (excess Ac2O). Kugelrohr distillation at 160 "C/0.05 mbar yielded 20.6 g oil (94 percent). Chiral GC: 10.3/10.6 min
 

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