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Chemical Structure| 96225-91-1 Chemical Structure| 96225-91-1

Structure of 96225-91-1

Chemical Structure| 96225-91-1

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Product Details of [ 96225-91-1 ]

CAS No. :96225-91-1
Formula : C9H14N4OS
M.W : 226.30
SMILES Code : NC1=NC(SC)=NC(N2CCOCC2)=C1

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Application In Synthesis of [ 96225-91-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 96225-91-1 ]

[ 96225-91-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 110-91-8 ]
  • [ 7440-44-0 ]
  • [ 1005-38-5 ]
  • [ 96225-91-1 ]
YieldReaction ConditionsOperation in experiment
In ethanol; hexane; benzene; EXAMPLE 35 A mixture of 5.2 g (0.02 mole) of <strong>[1005-38-5]4-amino-6-chloro-2-methylthiopyrimidine</strong> and 5.3 g (0.06 mole) of morpholine in 40 ml of ethanol was heated at reflux for fifteen hours. The mixture was then cooled and evaporated. The residue thereby obtained was diluted with water and extracted with dichloromethane. The extracts were dried over magnesium sulfate to provide a residue which was recrystallized with treatment with decolorizing charcoal from a benzene/hexane mixture to provide 4-amino-2-methylthio-6-(4-morpholino)pyrimidine, m.p. 125°-128° C. The structural assignment was supported by nuclear magnetic resonance spectral analysis.
 

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