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Chemical Structure| 96917-74-7 Chemical Structure| 96917-74-7

Structure of 96917-74-7

Chemical Structure| 96917-74-7

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Product Details of [ 96917-74-7 ]

CAS No. :96917-74-7
Formula : C26H19N
M.W : 345.44
SMILES Code : C1(N(C2=CC=CC=C2)C3=CC=CC=C3)=CC=C(C#CC4=CC=CC=C4)C=C1
MDL No. :N/A

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Application In Synthesis of [ 96917-74-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 96917-74-7 ]

[ 96917-74-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 13667-12-4 ]
  • [ 122-39-4 ]
  • [ 96917-74-7 ]
YieldReaction ConditionsOperation in experiment
80% With tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate; In toluene; at 90℃; for 12h;Inert atmosphere; General procedure: Under nitrogen protection,To a three-necked flask was added 100 ml of toluene,1 g of Intermediate 1 (2.99 mmol) prepared in Example 1,1.26 g of diphenylamine (7.45 mmol, 2.5 equ),0.90 g of sodium tert-butyl alcohol was added with stirring,59.8 mg of palladium acetate was added,0.5 mL of tri-tert-butylphosphine,90 C for 12 hours;The organic phase was extracted with dichloromethane,Spin dryTo give 1.30 g of product (P1) in 85% yield.
 

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