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Chemical Structure| 97962-11-3 Chemical Structure| 97962-11-3

Structure of 97962-11-3

Chemical Structure| 97962-11-3

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Product Details of [ 97962-11-3 ]

CAS No. :97962-11-3
Formula : C6H11BrO3
M.W : 211.05
SMILES Code : CC(OC)C(Br)C(OC)=O
MDL No. :MFCD24477053

Safety of [ 97962-11-3 ]

Application In Synthesis of [ 97962-11-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 97962-11-3 ]

[ 97962-11-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 67-56-1 ]
  • [ 17642-18-1 ]
  • [ 768-94-5 ]
  • [ 97962-11-3 ]
  • methyl (1-adamantan-1-yl)-3-methylaziridine-2-carboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
32%; 44% With triethylamine; at 20℃; under 4500450.0 Torr; for 17h; General procedure: The mixture of 1-aminoadamantane (151 mg, 1 mmol), Michael acceptor (3f-h) (2 mmol), and triethylamine (111 mg, 1.1 mmol) in solvent (2 mL) was placed in a Teflon reaction vessel and pressurized to 10 kbar at room temperature for the corresponding time. After that, the pressure was released and the mixture was concentrated in vacuo. The crude product was purified by column chromatography (Silica gel, pentane/ether, 9/1 (for 5d, 6a, 7), 7/3 (for 5e, 6b).
 

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