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Chemical Structure| 43141-69-1 Chemical Structure| 43141-69-1

Structure of 43141-69-1

Chemical Structure| 43141-69-1

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Product Details of [ 43141-69-1 ]

CAS No. :43141-69-1
Formula : C14H23NO
M.W : 221.34
SMILES Code : OC1=CC=CC(N(CCCC)CCCC)=C1
MDL No. :MFCD00134668
Boiling Point : No data available
InChI Key :KHSTZMGCKHBFJX-UHFFFAOYSA-N
Pubchem ID :601234

Safety of [ 43141-69-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319
Precautionary Statements:P264-P280-P302+P352+P332+P313+P362+P364-P305+P351+P338+P337+P313

Application In Synthesis of [ 43141-69-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 43141-69-1 ]

[ 43141-69-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 117-21-5 ]
  • [ 43141-69-1 ]
  • C36H46ClN2O3(1+)*Cl(1-) [ No CAS ]
YieldReaction ConditionsOperation in experiment
65% The following reactions were carried out under nitrogen flow. Add 9.1g (50.0mmol) of <strong>[117-21-5]3-chlorophthalic anhydride</strong> and 22.3g (360.0mmol) of N,N-dibutyl-3-aminophenol to a 300mL 4-necked flask equipped with condenser, stirring device and thermometer. After 80 mL of methanesulfonic acid and 50 mL of toluene, the mixture was stirred at 110C for 54 hours. After the reaction mixture was naturally cooled to room temperature (23-27C), it was poured into 1 L of ice water, and stirred at room temperature for 30 minutes. The mixture was filtered under reduced pressure, and the solid separated by filtration was dissolved in 100 mL of methanol and added dropwise to 1 L of a 1N aqueous hydrochloric acid solution. The solid obtained by filtering the mixture under reduced pressure was dried under reduced pressure at 80C overnight to obtain the following intermediate (102) (22.4 g, yield 65%).
 

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