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CAS No. : | 10025-83-9 | MDL No. : | MFCD00011063 |
Formula : | Cl3Ir | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | DANYXEHCMQHDNX-UHFFFAOYSA-K |
M.W : | 298.58 | Pubchem ID : | 25563 |
Synonyms : |
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Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P264-P280-P305+P351+P338-P337+P313 | UN#: | N/A |
Hazard Statements: | H319 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In methanol; | EXAMPLE 18 Into a stainless steel autoclave having an internal capacity of 40 ml, 0.48 g (5.0 mmol) of 3,5-dimethylpyrazole, 0.64 g (20 mmol) of methanol, 29.9 mg (2 mol %) of <strong>[10025-83-9]iridium trichloride</strong>, 125 mg (10 mol %) of tributyl phosphite and 10 ml of 1,4-dioxane were charged and reacted at 200 C. for 20 hours under a nitrogen pressure of 100 kg/cm2, whereby the yield of 1,3,5-trimethylpyrazole was 90.7%. |