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[ CAS No. 1004558-41-1 ] {[proInfo.proName]}

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Chemical Structure| 1004558-41-1
Chemical Structure| 1004558-41-1
Structure of 1004558-41-1 * Storage: {[proInfo.prStorage]}
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Product Details of [ 1004558-41-1 ]

CAS No. :1004558-41-1 MDL No. :MFCD13183456
Formula : C13H14ClNO2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 251.71 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 1004558-41-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1004558-41-1 ]

[ 1004558-41-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 53924-05-3 ]
  • [ 24424-99-5 ]
  • [ 1004558-41-1 ]
YieldReaction ConditionsOperation in experiment
94% With dmap; triethylamine In 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran at 20℃; for 11h;
75% With dmap In dichloromethane at 25℃; for 18h; Inert atmosphere;
With dmap In dichloromethane at 20℃; for 18h; 8.1 Example 8: r7-Chloro-2-(4-chloro-3-cvclohexylsulfamoyl-phenvD- 1 H-indol-3 -yll -acetic acidStep 1. Di-tert-butyi dicarbonate (7.92 g) is added to a solution of 7-chloroindole (5 g) and 4- (dimethylamino) pyridine (0.4 g) in DCM (165 mL). The reaction is stirred at room temperature for 18 hr. The reaction mixture is washed with IN HCl (100 mL) and IN NHCO3 (100 mL). The organic layer is separated, dried over MgSO4 and concentrated to afford 7^ chloro-indole-l-carboxylic acid tert-butyl ester as an oil (8.22 g).
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