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Chemical Structure| 101646-02-0 Chemical Structure| 101646-02-0

Structure of 101646-02-0

Chemical Structure| 101646-02-0

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Product Details of [ 101646-02-0 ]

CAS No. :101646-02-0
Formula : C7H2ClF4NO2
M.W : 243.54
SMILES Code : FC(C1=CC([N+]([O-])=O)=C(F)C(Cl)=C1)(F)F
MDL No. :MFCD00674108
Boiling Point : No data available
InChI Key :JVOKKJHIEVEFEB-UHFFFAOYSA-N
Pubchem ID :2736565

Safety of [ 101646-02-0 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H302+H332-H311-H315-H319
Precautionary Statements:P261-P264-P270-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P330-P361+P364-P405-P501
Class:6.1
UN#:2810
Packing Group:

Application In Synthesis of [ 101646-02-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 101646-02-0 ]

[ 101646-02-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 657-02-3 ]
  • [ 101646-02-0 ]
YieldReaction ConditionsOperation in experiment
67% With potassium fluoride; tetramethlyammonium chloride; (B) The 3-chloro-4-fluoro-5-nitrobenzotrifluoride starting reactant employed in the above example was prepared in the follow manner. A mixture of 52 parts of <strong>[657-02-3]3,4-dichloro-5-nitrobenzotrifluoride</strong>, 16.2 parts of anhydrous potassium fluoride and 2.5 parts of tetramethylammonium chloride was heated and maintained at about 120 to 140 C. for about 7 hours. The mixture was then cooled to room temperature, diluted with methylene chloride, and filtered. The filtrate was distilled to yield 35.2 parts (67% yield) of 3-chloro-4-fluoro-5-nitrobenzotrifluoride. The structure of the product was confirmed by gas chromatography-mass spectrum analysis.
 

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