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Chemical Structure| 1033705-64-4 Chemical Structure| 1033705-64-4

Structure of 1033705-64-4

Chemical Structure| 1033705-64-4

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Product Details of [ 1033705-64-4 ]

CAS No. :1033705-64-4
Formula : C13H24N2O3
M.W : 256.34
SMILES Code : O=C(N1C[C@@H](CNC(C)=O)CCC1)OC(C)(C)C

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Application In Synthesis of [ 1033705-64-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1033705-64-4 ]

[ 1033705-64-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 75-36-5 ]
  • [ 140645-23-4 ]
  • [ 1033705-64-4 ]
YieldReaction ConditionsOperation in experiment
100% With triethylamine; In dichloromethane; at 20℃; for 3h; (R)-3-(Acetylamino-methyl)-piperidine-1-carboxylic acid te/f-butyl esterTo a solution of 300 mg (1 ,4 mmol) (R)-3-aminomethyl-piperidine-1-carboxylic acid te/f-butyl ester in 10 ml methylene chloride is first added 370 mul (2,1 mmol) triethylamine and then slowly 0,110 ml (1 ,68 mmol) acetyl chloride. The reaction mixture is stirred at room temperature for three hours. Water is added afterwards. The organic phase is dried over sodium sulphate and concentrated.Yield: 370mg (103% of theory)EII Mass spectrum: m/z = 257 [M+H]+
 

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