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Chemical Structure| 1044598-80-2 Chemical Structure| 1044598-80-2

Structure of 1044598-80-2

Chemical Structure| 1044598-80-2

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Product Details of [ 1044598-80-2 ]

CAS No. :1044598-80-2
Formula : C46H72N2O2S2
M.W : 749.21
SMILES Code : O=C1N(C(C2=CC=CS2)=C3C(N(C(C4=CC=CS4)=C31)CC(CCCCCC)CCCCCCCC)=O)CC(CCCCCC)CCCCCCCC
MDL No. :MFCD29923947

Safety of [ 1044598-80-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338

Application In Synthesis of [ 1044598-80-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1044598-80-2 ]

[ 1044598-80-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1044598-80-2 ]
  • [ 74137-36-3 ]
  • 6,6'-((5-methoxy-1,3-phenylene)bis(thiophene-5,2-diyl))bis(2,5-bis(2-hexyldecyl)-3-(thiophen-2-yl)pyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione) [ No CAS ]
YieldReaction ConditionsOperation in experiment
90.80 mg With tris-(dibenzylideneacetone)dipalladium(0); tris(o-methoxyphenyl)phosphine; caesium carbonate; Trimethylacetic acid; In toluene; at 100℃; for 24h;Schlenk technique; Inert atmosphere; General procedure: Typically, TDPP (200 mg, 0.27 mmol), dibromobenzene derivatives 0.11 mmol, anhydrous Cs2CO3(200 mg, 0.61 mmol), PivOH (7.9 mg, 0.08 mmol), Pd2(dba)3 (4.00 mg, 1.5 mol%), tris(o-methoxyphenyl)phosphine (3.08 mg, 3 mol%) were successively added into a Schlenk tube. The tube was purged by three repetitions of vacuum and argon filling. Then, 5 mL anhydrous toluene was added via syringe.The reaction solution was deoxygenated using three freeze-vacuum-thaw cycles, and then rigorouslystirred at 100 C for 24 h under argon atmosphere. Removal of the toluene by rotary evaporatoraorded the crude product, which was then purified by chromatogragh column (CC) on silica gelusing a mixture of CH2Cl2 and hexane as eluent, giving the target molecules Ms1~9.
 

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