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[ CAS No. 104566-43-0 ] {[proInfo.proName]}

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Type HazMat fee for 500 gram (Estimated)
Excepted Quantity USD 0.00
Limited Quantity USD 15-60
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Chemical Structure| 104566-43-0
Chemical Structure| 104566-43-0
Structure of 104566-43-0 * Storage: {[proInfo.prStorage]}
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Product Details of [ 104566-43-0 ]

CAS No. :104566-43-0 MDL No. :MFCD07786725
Formula : C14H15NO Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 213.28 Pubchem ID :-
Synonyms :

Safety of [ 104566-43-0 ]

Signal Word:Danger Class:6.1
Precautionary Statements:P261-P280-P305+P351+P338-P311 UN#:3439
Hazard Statements:H302+H312-H315-H319-H331-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 104566-43-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 104566-43-0 ]
  • Downstream synthetic route of [ 104566-43-0 ]

[ 104566-43-0 ] Synthesis Path-Upstream   1~1

  • 1
  • [ 104566-43-0 ]
  • [ 104566-41-8 ]
YieldReaction ConditionsOperation in experiment
79% With hydrogenchloride In dichloromethane at 20℃; for 1 h; To the compound (1.6 g, 7.6 mmol) obtained in step 204 2 was added 3 mol/L 206 hydrogen chloride(dichloromethane solution, 5 mL), and the mixture was stirred at room temperature for 1 hr, and concentratedunder reduced pressure to give the 207 title compound ( 1.5 g , 6.0 mmol, 79percent). MS(ESI) m/z 214 (M+H)+ 1H NMR (400 MHz, CD3OD): δ7.47-7.30 (m, 6H), 7.09 (s, 1H), 7.01-6.99 (m, 2H), 5.12 (s, 2H), 3.95 (s,2H) .
Reference: [1] Patent: US2016/332999, 2016, A1, . Location in patent: Paragraph 0407; 0408; 0409
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