There will be a HazMat fee per item when shipping a dangerous goods. The HazMat fee will be charged to your UPS/DHL/FedEx collect account or added to the invoice unless the package is shipped via Ground service. Ship by air in Excepted Quantity (each bottle), which is up to 1g/1mL for class 6.1 packing group I or II, and up to 25g/25ml for all other HazMat items.
Type | HazMat fee for 500 gram (Estimated) |
Excepted Quantity | USD 0.00 |
Limited Quantity | USD 15-60 |
Inaccessible (Haz class 6.1), Domestic | USD 80+ |
Inaccessible (Haz class 6.1), International | USD 150+ |
Accessible (Haz class 3, 4, 5 or 8), Domestic | USD 100+ |
Accessible (Haz class 3, 4, 5 or 8), International | USD 200+ |
Purity | Size | Price | VIP Price | USA Stock *0-1 Day | Global Stock *5-7 Days | Quantity | |||||
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CAS No. : | 10465-82-4 | MDL No. : | MFCD00043006 |
Formula : | C10H16N4O4 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 256.26 | Pubchem ID : | - |
Synonyms : |
|
Signal Word: | Danger | Class: | 4.1 |
Precautionary Statements: | P261-P210-P264-P280-P370+P378-P302+P352+P312 | UN#: | 1325 |
Hazard Statements: | H302+H312+H332-H315-H319-H228 | Packing Group: | Ⅲ |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
55% | at 0 - 20℃; for 5 h; | To a stirred solution of diethyl azodicarboxylate(40 wtpercent in toluene; 5 mL, 11.5 mmol, 1 equiv) in Et2O (25 mL) at 0 C wasadded a solution of morpholine (1.98 mL, 23 mmol, 2 equiv) in Et2O (25 mL)over 3 h with a dropping funnel. The reaction mixture was stirred for afurther 2 h whilst slowing warming to room temperature. The yelloworangeprecipitate was collected by vacuum filtration, washed with coldEt2O, and dried on the filter to furnish ADDM as a yellow-orange solid (1.62 g,55percent yield): dH (CDCl3, 400 MHz) 3.61 (m, 4H, 2CH2), 3.74 (m, 8H, 4CH2), 3.83(m, 4H, 2CH2). |
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