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Chemical Structure| 10505-25-6 Chemical Structure| 10505-25-6

Structure of 10505-25-6

Chemical Structure| 10505-25-6

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Product Details of [ 10505-25-6 ]

CAS No. :10505-25-6
Formula : C6H6N4O2
M.W : 166.14
SMILES Code : O=C(N1)C2=CN(C)N=C2NC1=O
MDL No. :MFCD16620718

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Application In Synthesis of [ 10505-25-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 10505-25-6 ]

[ 10505-25-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 21230-43-3 ]
  • [ 57-13-6 ]
  • [ 10505-25-6 ]
YieldReaction ConditionsOperation in experiment
95% at 200℃; for 2h; Compound 297; 2-Methyl-2,7-dihydropyrazolo[3,4-d]pyrimidine-4,6-dione; Compound 296 (2 g, 11.8 mmol) was melted at 200 C. with 6 g urea (large excess) for two hours. The reaction was permitted to cool to 40 C. and 20 mL water was added. The mixture was then boiled for 1 hour and stirred at room temperature overnight. Filtration and drying in vacuo afforded 1.86 g (95%) of a white solid. Compound 297: mp >300 C.; MS (ES+calculated: 166.14; found: 167.24 M+H). HPLC (100% purity, retention time 2.103 minutes-Method A); 1H NMR (400 MHz, DMSO-d6): 6 11.34 (br s, 1H), 10.66 (br s, 1H), 8.27 (s, 1H), 3.82 (s, 3H).
 

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