Home Cart Sign in  
Chemical Structure| 105194-22-7 Chemical Structure| 105194-22-7

Structure of 105194-22-7

Chemical Structure| 105194-22-7

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 105194-22-7 ]

CAS No. :105194-22-7
Formula : C13H13NO3
M.W : 231.25
SMILES Code : O=C(C(C1)=C(C2=CC=CC=C2)NC1=O)OCC
MDL No. :MFCD10511535

Safety of [ 105194-22-7 ]

Application In Synthesis of [ 105194-22-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 105194-22-7 ]

[ 105194-22-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 7310-97-6 ]
  • [ 105194-22-7 ]
  • C36H32N2O8 [ No CAS ]
YieldReaction ConditionsOperation in experiment
50% With toluene-4-sulfonic acid; acetic acid; at 60 - 100℃; for 3h; 5-Phenyl-4-carbethoxy-1, 3-DIHYDRO-PYRROL-2-ONE (2.3 g, 0.01 mol) is dissolved in acetic acid (50 ML) at 60 to 70 C. To this PTSA (0.7 g) is added, followed by addition of 2, 5-dimethoxy- terephthalaldehyde (1. 0 g, 0.005 mol) and temperature is increased to 100 C. Heating is continued for 3 hours and after cooling, solids are filtered through Buchner funnel. The crude product is washed with acetic acid, water, DMF and methanol. Finally the crude product is dissolved in conc. sulphuric acid, reprecipitated from water and filtered. It is then dried in an oven to give red colored pure product (1.5 g, 50%). Anal. CALC. FOR C3GH32N208 ; C, 69. 60; H, 5.15 ; N, 4.52 ; Found: C, 66.47 ; H, 4.98 ; N, 4.34. All other compounds given in the Table 6 are obtained following the above same procedure
 

Historical Records