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CAS No. : | 10543-12-1 | MDL No. : | MFCD00016515 |
Formula : | C10H10O5 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | WTPDKEAYVAXNRO-UHFFFAOYSA-N |
M.W : | 210.18 | Pubchem ID : | 66346 |
Synonyms : |
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Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P280-P301+P312-P302+P352-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
74% | 0.25g (1.2mmol) 4-acetoxy-3-methoxybenzoic acid, 0.16g (1.2mmol) 1-hydroxybenzotriazole, 0.23g (1.2mmol) 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride was dissolved in 10mL N,N-dimethylformamide and stirred for 30 min, Add 0.19g (1mmol) 2-amino-4-methylthiazole-5-carboxylic acid ethyl ester, reaction at 115C for 10h (TLC monitoring), The reaction solution was cooled to room temperature, Pour into ice water, separate out solids, filter with suction, Use saturated sodium bicarbonate solution, Wash with dilute hydrochloric acid and water, Dry to obtain off-white powder N-(5-ethoxycarbonyl-4-methylthiazol-2-yl)-4-acetoxy-3-methoxybenzamide, The yield is 74.0%, m.p. 195~197C. |