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CAS No. : | 105618-29-9 | MDL No. : | N/A |
Formula : | C18N6O9 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | BTASSOQNDRGAGE-UHFFFAOYSA-N |
M.W : | 444.23 | Pubchem ID : | 13692981 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P280-P301+P312-P302+P352-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Yield given; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
88% | In acetonitrile |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In N,N-dimethyl acetamide for 0.25h; Heating; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With trifluoroacetic anhydride |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Title compound not separated from byproducts; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
95% | With acetic anhydride at 115℃; for 0.166667h; | |
With acetic anhydride at 115℃; | ||
With acetic anhydride at 115 - 117℃; for 0.333333h; Inert atmosphere; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In acetonitrile |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In acetonitrile for 1h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: acetonitrile 2: thionyl chloride / 0.5 h / Heating |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 3 steps 1: acetonitrile 2: thionyl chloride / 0.5 h / Heating 3: 0.25 h |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 4 steps 1: acetonitrile 2: thionyl chloride / 0.5 h / Heating 3: 0.25 h 4: 60 percent / acetonitrile / 0.17 h / Heating |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
7% | Stage #1: hexaazatriphenylenehexacarboxylic acid trianhydride; 4,5-bis(octyloxy)benzene-1,2-diamine With triethylamine In acetonitrile at 90℃; for 24h; Inert atmosphere; Stage #2: In 1-methyl-pyrrolidin-2-one at 190℃; for 30h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Stage #1: hexaazatriphenylenehexacarboxylic acid trianhydride; 4,5-bis(octyloxy)benzene-1,2-diamine With triethylamine In acetonitrile at 90℃; for 24h; Inert atmosphere; Stage #2: In 1-methyl-pyrrolidin-2-one at 190℃; for 30h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 3 steps 1.1: sulfuric acid / 72 h / 20 °C 2.1: acetic acid; sodium nitrite; trifluoroacetic acid / 12 h 2.2: 12 h / 20 °C 3.1: acetic anhydride / 0.33 h / 115 - 117 °C / Inert atmosphere |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1.1: acetic acid; sodium nitrite; trifluoroacetic acid / 12 h 1.2: 12 h / 20 °C 2.1: acetic anhydride / 0.33 h / 115 - 117 °C / Inert atmosphere |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
89.3 % | With ammonium hydroxide at 20℃; Inert atmosphere; | 1-7 Example 1 General procedure: Add 30ml of ammonia (28wt%) to a 100mL three-mouth flask, and at the same time add hexaazabenzophenanthrene hexacarboxylic acid trianhydride (purchased from Aneji) (0.444g, 1mmol), under the protection of nitrogen, the reaction mixture is subjected to uninterrupted magnetic stirring at room temperature, the reaction time is 6 hours, after the end of the reaction, vacuum filtration collects solids, washed with ethanol three times, and vacuum drying at 60 °C overnight to obtain compound A: hexaazabenzophanthrene hexaforminimide, with a yield of 85.8%. |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
80.5 % | In N,N-dimethyl-formamide Inert atmosphere; Reflux; | 8-13 Example 8 General procedure: Add 45 mL of anhydrous DMF to a 100 ml three-mouth flask and purge with nitrogen for 15 min while adding hexaazabenzophene hexacarboxylic acid trianhydride (0.444 g, 1 mmol) and 3,5-diamino-1,2,4-triazole (0.396 g, 4 mmol). In the whole process, under the protection of nitrogen, continuous stirring and heating reflux for 24 hours, then the heating device was removed to cool to room temperature, the solid product was precipitated through an ice water bath, the solids were collected by filtration, the filter cake was washed three times with ethanol, and vacuum dried to obtain compound B: tris(3-amino-1,2,4-triazolyl)hexaazabenzophenanthrene hexaformylimide with a yield of 75.2%. |
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