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Chemical Structure| 1061682-78-7 Chemical Structure| 1061682-78-7

Structure of 1061682-78-7

Chemical Structure| 1061682-78-7

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Product Details of [ 1061682-78-7 ]

CAS No. :1061682-78-7
Formula : C12H25N3O2
M.W : 243.35
SMILES Code : O=C(N1CC(NC)(NC)CCC1)OC(C)(C)C
MDL No. :MFCD09878593

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Application In Synthesis of [ 1061682-78-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1061682-78-7 ]

[ 1061682-78-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 940890-90-4 ]
  • [ 124-40-3 ]
  • [ 1061682-78-7 ]
YieldReaction ConditionsOperation in experiment
99% In methanol; at 90℃; for 48h;Sealed tube; Method N: (R)-tert-butyl 3-(dimethylamino)piperidine-1-carboxylate A solution of (S)-tert-butyl 3-(methylsulfonyloxy)piperidine-1-carboxylate (1.0 g, 3.58 mmol) and 2 M dimethylamine in methanol (60 ml) was placed in a sealed tube and heated to 90° C. for 48 hours. The reaction mixture was allowed to cool down to room temperature and was concentrated in vacuo. Ethyl acetate was added to the residue. The remaining mesylate crashed out and was removed by filtration. The filtrate was concentrated in vacuo to give the desired compound as a sticky orange oil (0.808 g, 99percent yield).
 

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