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Chemical Structure| 1068155-22-5 Chemical Structure| 1068155-22-5

Structure of 1068155-22-5

Chemical Structure| 1068155-22-5

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Product Details of [ 1068155-22-5 ]

CAS No. :1068155-22-5
Formula : C10H15BO3
M.W : 194.04
SMILES Code : OC1=CC(C(C)(C)C)=CC=C1B(O)O

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Application In Synthesis of [ 1068155-22-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1068155-22-5 ]

[ 1068155-22-5 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 6287-82-7 ]
  • [ 1068155-22-5 ]
  • 2-(3-bromobenzo[b]thiophene-2-yl)-5-(tert-butyl)phenol [ No CAS ]
YieldReaction ConditionsOperation in experiment
76% With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In 1,4-dioxane; water; at 90℃; for 6h;Schlenk technique; 1) accurate weighing 2, 3 - b bromophenylacetic and [b] Thiophene (300 mg, 1.0 mmol), 4 - tert butyl -2 - hydroxy phenyl boronic acid (300 mg, 1.5 mmol), and in turn to 25 ml of in shu Lunke bottle, adding potassium carbonate (3.0 equivalent), four (triphenylphosphine) palladium (5% mol), 1, 4 - dioxane/water (volume ratio 4:1), is 90 C reaction in oil bath 6 hours. After the reaction, the solvent is removed under reduced pressure, the use of silica gel column separation, petroleum ether/ethyl acetate as eluant, to obtain 2 - (3 - bromo - benzo [b] Thiophene -2 - yl) -5 - tertiary butyl phenol 3d, and the yield is 76%.1
  • 2
  • [ 6287-82-7 ]
  • [ 1068155-22-5 ]
  • 7-(tert-butyl)benzo[4,5]thieno[3,2-b]benzofuran [ No CAS ]
 

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