Home Cart Sign in  
Chemical Structure| 1072836-76-0 Chemical Structure| 1072836-76-0

Structure of 1072836-76-0

Chemical Structure| 1072836-76-0

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 1072836-76-0 ]

CAS No. :1072836-76-0
Formula : C14H17N3O4S2
M.W : 355.43
SMILES Code : O=S(=O)(NS(=O)(=O)C1=CC(N)=CC=C1C)C2=CC(N)=CC=C2C
MDL No. :N/A

Safety of [ 1072836-76-0 ]

Application In Synthesis of [ 1072836-76-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1072836-76-0 ]

[ 1072836-76-0 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 444731-75-3 ]
  • [ 1072836-76-0 ]
  • C42H43N13O4S2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
78.8% In methanol; for 3h;Reflux; Amino 3 (1.90 g, 5.35 mmol)Chloride (compound VI, 3.24g, 10.22mmol) and methanol (150mml) were added and heated to reflux for 3h.Was added HCl-dioxane solution (0.1mml); the solvent was evaporated under reduced pressure to give a solid, the solid was added methanol (50ml), heated to reflux, partially dissolved,Filtered while still hot to obtain a solid dimer (Compound I)3.62g, 78.8% yield, purity 98%.
  • 2
  • [ 444731-75-3 ]
  • [ 1072836-76-0 ]
  • C42H43N13O4S2*2ClH [ No CAS ]
YieldReaction ConditionsOperation in experiment
0.16 g With hydrogenchloride; In isopropyl alcohol; for 3h;Reflux; The residue above was dissolved in 50 mL iPrOH, followed by addition of IM2 (2.13 g, 7.4 mmol) and 0.5 mL conc HCl. The mixture was stirred for 3h at reflux temperature. After cooling, the reaction mixture was concentrated under reduced pressure. 0.16 g (overall yield 5.1%) compound was obtained as a yellow solid after purification by flash column chromatography (CH2Cl2/CH3OH) on silica gel. 1H NMR (500 MHz, DMSO-d6) (delta, ppm): 10.89 (brs, 2H), 8.12 - 8.22 (m, 2H), 7.86 (d, J = 8.7 Hz, 2H), 7.76 - 7.80 (m, 2H), 7.62 - 7.68 (m, 2H), 7.42 - 7.50 (m, 2H), 7.12-7.15 (m, 2H), 6.97 (d, J = 8.7 Hz, 2H), 5.70 - 5.78 (m, 2H), 4.09 (s, 6H),3.55 (s, 6H), 2.64 (s, 6H), 2.41 (s, 6H). 13C NMR (600 MHz, DMSO-d6) (delta, ppm): 162.4, 151.0, 146.5, 143.9, 142.6, 140.4, 134.5, 133.8, 133.6, 131.9, 123.3, 121.7, 120.6, 120.2, 118.9, 114.6, 96.3, 37.9, 19.8, 9.9; HRMS m/z calcd for C42H44N13O4S2[M+H]+ 858.3075, found 858.3082.
 

Historical Records