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Structure of 1072945-06-2

Chemical Structure| 1072945-06-2

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Product Details of [ 1072945-06-2 ]

CAS No. :1072945-06-2
Formula : C13H18BNO4
M.W : 263.10
SMILES Code : O=[N+](C1=CC(B2OC(C)(C)C(C)(C)O2)=CC=C1C)[O-]
MDL No. :MFCD09027080
InChI Key :XYZOZOWGODLRCW-UHFFFAOYSA-N
Pubchem ID :46738770

Safety of [ 1072945-06-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 1072945-06-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1072945-06-2 ]

[ 1072945-06-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 76-09-5 ]
  • [ 80500-27-2 ]
  • [ 1072945-06-2 ]
YieldReaction ConditionsOperation in experiment
81% With 1H-imidazole; iron(III) chloride; In water; acetonitrile; at 20℃; for 0.5h;Inert atmosphere; General procedure: To a solution of aryl boronic acid (1 mmol) in MeCN (4 mL) was added, sequentially, asolution of FeCl3 (8 mg, 0.05 mmol, 5 mol%) in H2O (1 mL), imidazole (204 mg, 3 mmol)and pinacol (118 mg, 1 mmol). The resulting cloudy orange mixture was stirred at roomtemperature for 30 min. The reaction was then diluted with H2O (5 mL) and extracted withEt2O (3 x 8 mL). The combined organic extracts were dried (Na2SO4) and concentrated invacuo. The resulting oil was then purified by a filtration through a silica gel plug (eluting withEt2O), affording the title compound.
 

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